Pentanal, 2-[(4-methylphenyl)hydrazono]-3-oxo-, (2E)- (9CI)

Base Information

Chemical Name:Pentanal, 2-[(4-methylphenyl)hydrazono]-3-oxo-, (2E)- (9CI)
CAS No.:810672-44-7
Molecular Formula:C₁₂H₁₄N₂O₂
Molecular Weight:218.255
Hs Code.:
Mol file:810672-44-7.mol

Synonyms:Pentanal,2-[(4-methylphenyl)hydrazono]-3-oxo-, (2E)- (9CI)

Suppliers and Price of Pentanal, 2-[(4-methylphenyl)hydrazono]-3-oxo-, (2E)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Pentanal, 2-[(4-methylphenyl)hydrazono]-3-oxo-, (2E)- (9CI)

Chemical Property:

PSA：58.53000
LogP:2.01390

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Pentanal, 2-[(4-methylphenyl)hydrazono]-3-oxo-, (2E)- (9CI)

There total 2 articles about Pentanal, 2-[(4-methylphenyl)hydrazono]-3-oxo-, (2E)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 6137-82-2,38664-62-9
(E)-1-(N,N-dimethylamino)-1-penten-3-one

: 540-23-8
p-toluidine hydrochloride

: 810672-44-7
3-oxo-2-(p-tolylhydrazono)pentanal

Guidance literature:: p-toluidine hydrochloride; With sodium nitrite; In water;

(E)-1-(N,N-dimethylamino)-1-penten-3-one; With sodium acetate; In ethanol; at 20 ℃; for 0.5h;
DOI:10.1002/jhet.5570410501

Reference yield: 72.0%

: 6137-82-2,38664-62-9
(E)-1-(N,N-dimethylamino)-1-penten-3-one

: 540-23-8
p-toluidine hydrochloride

: 810672-44-7
3-oxo-2-(p-tolylhydrazono)pentanal

Guidance literature:: p-toluidine hydrochloride; With sodium nitrite; cooling;

(E)-1-(N,N-dimethylamino)-1-penten-3-one; With sodium acetate; In ethanol; water; at 20 ℃; for 0.5h;

Reference yield:

: 810672-44-7
3-oxo-2-(p-tolylhydrazono)pentanal

: 810672-70-9
5-ethyl-4-(4-methylphenylazo)isoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / hydroxylamine hydrochloride; sodium carbonate / 0.08 h / Irradiation

2: 67 percent / acetic anhydride / 4 h / Heating

With hydroxylamine hydrochloride; acetic anhydride; sodium carbonate;
DOI:10.1002/jhet.5570410501