racemic O-acetyl-N-(2-iodobenzyl)-N-methyl-β-(2-iodophenyl)ethanolamine

Base Information

Chemical Name:racemic O-acetyl-N-(2-iodobenzyl)-N-methyl-β-(2-iodophenyl)ethanolamine
CAS No.:118162-24-6
Molecular Formula:C₁₈H₁₉I₂NO₂
Molecular Weight:535.163
Hs Code.:

Synonyms:racemic O-acetyl-N-(2-iodobenzyl)-N-methyl-β-(2-iodophenyl)ethanolamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of racemic O-acetyl-N-(2-iodobenzyl)-N-methyl-β-(2-iodophenyl)ethanolamine

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Technology Process of racemic O-acetyl-N-(2-iodobenzyl)-N-methyl-β-(2-iodophenyl)ethanolamine

There total 4 articles about racemic O-acetyl-N-(2-iodobenzyl)-N-methyl-β-(2-iodophenyl)ethanolamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 108-24-7
acetic anhydride

: 118162-20-2
racemic N-(iodobenzyl)-N-methyl-β-(2-iodophenyl)ethanolamine

: 118162-24-6
racemic O-acetyl-N-(2-iodobenzyl)-N-methyl-β-(2-iodophenyl)ethanolamine

Guidance literature:: for 48h; Ambient temperature;
DOI:10.1002/jhet.5570250123

Reference yield:

: 26260-02-6
2-iodobenzaldehyde

: 118162-24-6
racemic O-acetyl-N-(2-iodobenzyl)-N-methyl-β-(2-iodophenyl)ethanolamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaHCO₃, 2) NaBH₄ / 1) ethanol, reflux, 2 h, 2) reflux, 2 h

2: 1) boric acid, 2) NaBH₄ / 1) CH₃OH, r.t., 5 min, 2) 30 min

3: 98 percent / 48 h / Ambient temperature

With sodium tetrahydroborate; boric acid; sodium hydrogencarbonate;
DOI:10.1002/jhet.5570250123

Reference yield:

: 118162-19-9
N-(2-iodobenzyl)-β-(2-iodophenyl)ethanolamine

: 118162-24-6
racemic O-acetyl-N-(2-iodobenzyl)-N-methyl-β-(2-iodophenyl)ethanolamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1) boric acid, 2) NaBH₄ / 1) CH₃OH, r.t., 5 min, 2) 30 min

2: 98 percent / 48 h / Ambient temperature

With sodium tetrahydroborate; boric acid;
DOI:10.1002/jhet.5570250123