4-benzyloxymethyl-5-(2-chloroethyl)-3-(3-chloropropyl)-6-methylsalicylic acid methyl ester

Base Information

Chemical Name:4-benzyloxymethyl-5-(2-chloroethyl)-3-(3-chloropropyl)-6-methylsalicylic acid methyl ester
CAS No.:1206891-96-4
Molecular Formula:C₂₂H₂₆Cl₂O₄
Molecular Weight:425.352
Hs Code.:

Synonyms:4-benzyloxymethyl-5-(2-chloroethyl)-3-(3-chloropropyl)-6-methylsalicylic acid methyl ester

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Chemical Property of 4-benzyloxymethyl-5-(2-chloroethyl)-3-(3-chloropropyl)-6-methylsalicylic acid methyl ester

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Technology Process of 4-benzyloxymethyl-5-(2-chloroethyl)-3-(3-chloropropyl)-6-methylsalicylic acid methyl ester

There total 1 articles about 4-benzyloxymethyl-5-(2-chloroethyl)-3-(3-chloropropyl)-6-methylsalicylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1042721-68-5
1-acetyl-1-(benzyloxymethyl)carbonylcyclopropane

: 1071146-53-6
7-chloro-1-methoxy-1,3-bis(trimethylsilyloxy)-1,3-heptadiene

: 1206891-96-4
4-benzyloxymethyl-5-(2-chloroethyl)-3-(3-chloropropyl)-6-methylsalicylic acid methyl ester

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -78 - 20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1021/jo902334q

Reference yield: 79.0%

: 1206891-96-4
4-benzyloxymethyl-5-(2-chloroethyl)-3-(3-chloropropyl)-6-methylsalicylic acid methyl ester

: 1206892-07-0
5-(2-chloroethyl)-3-(3-chloropropyl)-4-hydroxymethyl-6-methylsalicylic acid methyl ester

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/jo902334q

Reference yield: 73.0%

: 1206891-96-4
4-benzyloxymethyl-5-(2-chloroethyl)-3-(3-chloropropyl)-6-methylsalicylic acid methyl ester

: 1206892-20-7
5-benzyloxymethyl-6-(2-chloroethyl)-7-methyl-chromane-8-carboxylic acid methyl ester

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at -78 - -23 ℃; Inert atmosphere;
DOI:10.1021/jo902334q