(-)-PD 135385

Base Information

Chemical Name:(-)-PD 135385
CAS No.:142507-52-6
Molecular Formula:C₂₃H₂₉N₃
Molecular Weight:347.503
Hs Code.:

Synonyms:(-)-PD 135385

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Chemical Property of (-)-PD 135385

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Technology Process of (-)-PD 135385

There total 10 articles about (-)-PD 135385 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 142437-99-8
(S)-1-<(4-phenyl-3-cyclohexen-1-yl)acetyl>-4-(2-pyridinyl)piperazine

: 142507-52-6
(-)-PD 135385

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; for 4h; Heating;
DOI:10.1021/jo00043a038

Reference yield:

: 34803-66-2
1-(2-pyridyl)piperazine

: 142507-52-6
(-)-PD 135385

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) CH₂Cl₂, ice bath, 15 min, 2.) to r. t., 1 h

2: 88 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 4 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00043a038

Reference yield:

: (S)-3-(2-Hydroxy-ethyl)-6-oxo-6-phenyl-hexanoic acid ethyl ester

: 142507-52-6
(-)-PD 135385

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran; H₂O / 0.25 h / Heating

2: 11.7 g / dimethylsulfoxide / 2 h / 160 °C

3: 65 percent / NaH / dimethylsulfoxide / 1.5 h / 19 - 22 °C

4: CH₂Cl₂ / 1 h / 0 °C

5: 1.) CH₂Cl₂, ice bath, 15 min, 2.) to r. t., 1 h

6: 88 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 4 h / Heating

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/jo00043a038