p-methoxyphenyl 6-O-benzyl-2-deoxy-3-O-levulinoyl-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl 6-O-benzyl-2-deoxy-3-O-levulinoyl-2-phthalimido-β-D-glucopyranoside
CAS No.:277310-66-4
Molecular Formula:C₃₃H₃₃NO₁₀
Molecular Weight:603.626
Hs Code.:

Synonyms:p-methoxyphenyl 6-O-benzyl-2-deoxy-3-O-levulinoyl-2-phthalimido-β-D-glucopyranoside

Suppliers and Price of p-methoxyphenyl 6-O-benzyl-2-deoxy-3-O-levulinoyl-2-phthalimido-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methoxyphenyl 6-O-benzyl-2-deoxy-3-O-levulinoyl-2-phthalimido-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of p-methoxyphenyl 6-O-benzyl-2-deoxy-3-O-levulinoyl-2-phthalimido-β-D-glucopyranoside

There total 4 articles about p-methoxyphenyl 6-O-benzyl-2-deoxy-3-O-levulinoyl-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: p-methoxyphenyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-phthalimido-β-D-glucopyranoside

: 277310-66-4
p-methoxyphenyl 6-O-benzyl-2-deoxy-3-O-levulinoyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; for 3.5h; cooling;
DOI:10.1021/ja062531e

Reference yield:

: C₃₃H₃₁NO₁₀

: 277310-66-4
p-methoxyphenyl 6-O-benzyl-2-deoxy-3-O-levulinoyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With triethylsilane; trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1016/j.tet.2020.131412

Reference yield:

: 138906-43-1
4-methoxyphenyl 4,6-di-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 277310-66-4
p-methoxyphenyl 6-O-benzyl-2-deoxy-3-O-levulinoyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; diisopropyl-carbodiimide / dichloromethane / 5 h / 20 °C

2: triethylsilane; trifluorormethanesulfonic acid / dichloromethane / 3 h / 0 °C

With triethylsilane; dmap; trifluorormethanesulfonic acid; diisopropyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.tet.2020.131412