4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenyl 4-decyloxybenzoate

Base Information

Chemical Name:4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenyl 4-decyloxybenzoate
CAS No.:1451058-62-0
Molecular Formula:C₃₄H₄₈N₄O₃
Molecular Weight:560.78
Hs Code.:

Synonyms:4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenyl 4-decyloxybenzoate

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Chemical Property of 4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenyl 4-decyloxybenzoate

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Technology Process of 4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenyl 4-decyloxybenzoate

There total 5 articles about 4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenyl 4-decyloxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 5519-23-3
p-decyloxybenzoic acid

: 1451058-54-0
4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenol

: 1451058-62-0
4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenyl 4-decyloxybenzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1039/c3tc30966e

Reference yield:

: 767-00-0
4-cyanophenol

: 1451058-62-0
4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenyl 4-decyloxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 24 h / 120 °C

2.1: sodium hydroxide / water / 0.5 h / Cooling with ice

3.1: potassium carbonate / acetone / 48 h / Reflux

4.1: potassium hydroxide / water; methanol / 12 h / Reflux

4.2: pH 2 / Cooling with ice

5.1: dicyclohexyl-carbodiimide; dmap / tetrahydrofuran / 24 h / 20 °C

With dmap; sodium azide; potassium carbonate; ammonium chloride; dicyclohexyl-carbodiimide; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c3tc30966e

Reference yield:

: 1451058-52-8
4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenyl acetate

: 1451058-62-0
4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenyl 4-decyloxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / water; methanol / 12 h / Reflux

1.2: pH 2 / Cooling with ice

2.1: dicyclohexyl-carbodiimide; dmap / tetrahydrofuran / 24 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; potassium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1039/c3tc30966e