1-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

Base Information

• Chemical Name: 1-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester
• CAS No.: 838821-81-1
• Molecular Formula: C₂₃H₂₃F₅O₁₁S
• Molecular Weight: 602.487

Synonyms:1-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

Chemical Property of 1-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

There total 2 articles about 1-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-glucose pentaacetate (83-87-4,604-68-2,604-69-3,2152-77-4,4026-35-1,4163-59-1,4163-60-4,4163-61-5,4163-65-9,4257-94-7,4257-96-9,16299-15-3,19186-39-1,19189-55-0,25878-60-8,25941-03-1,32445-48-0,32445-49-1,32445-53-7,32445-54-8,34685-58-0,34685-59-1,43168-42-9,43168-44-1,43169-22-8,43169-25-1,66966-07-2,70749-17-6,80184-01-6,93221-01-3,93221-02-4,99630-88-3,109215-53-4,115792-70-6,115792-73-9,139894-92-1,139973-25-4,144071-49-8,147648-81-5) → 1-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester (838821-81-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / BF₃*OEt₂ / CH₂Cl₂ / 4 h / 20 °C

2: N,N'-diisopropylcarbodiimide / tetrahydrofuran / 24 h

With boron trifluoride diethyl etherate; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jm040794i

Reference yield:

S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid (3254-10-2) + 2,3,4,5,6-pentafluorophenol (771-61-9) → 1-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester (838821-81-1)

Guidance literature:

With diisopropyl-carbodiimide; In tetrahydrofuran; for 24h;

DOI:10.1021/jm040794i

Reference yield:

1-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester (838821-81-1) + C59H75IN10O14S2 → C76H97IN10O24S3

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1021/jm040794i

upstream raw materials:

S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid

2,3,4,5,6-pentafluorophenol

D-glucose pentaacetate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 838821-81-1 1-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3-mercaptopropionic acid pentafluorophenyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send