Technology Process of 3-<2-methoxy-4-(methoxymethoxy)phenyl>propanal
There total 5 articles about 3-<2-methoxy-4-(methoxymethoxy)phenyl>propanal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
for 2h;
DOI:10.1021/jo00347a032
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 98 percent / 10percent aq. NaOH, methyltrialkyl(C8-C10)ammonium chloride (Adogen 464) / CH2Cl2 / 2 h
2: 97 percent / H2 / 10percent Pd/C / 24 h / 775.7 Torr
3: 96 percent / K2CO3 / acetone / 5 h / Heating
4: 94 percent / LiAlH4 / diethyl ether / 4 h / Heating
5: 92 percent / pyridinium chlorochromate / CH2Cl2 / 2 h
With
sodium hydroxide; lithium aluminium tetrahydride; methyltrialkyl(C8-C10)ammonium chloride (Adogen 464); hydrogen; potassium carbonate; pyridinium chlorochromate;
palladium on activated charcoal;
In
diethyl ether; dichloromethane; acetone;
DOI:10.1021/jo00347a032
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 97 percent / H2 / 10percent Pd/C / 24 h / 775.7 Torr
2: 96 percent / K2CO3 / acetone / 5 h / Heating
3: 94 percent / LiAlH4 / diethyl ether / 4 h / Heating
4: 92 percent / pyridinium chlorochromate / CH2Cl2 / 2 h
With
lithium aluminium tetrahydride; hydrogen; potassium carbonate; pyridinium chlorochromate;
palladium on activated charcoal;
In
diethyl ether; dichloromethane; acetone;
DOI:10.1021/jo00347a032
