(E)-3-phenoxy-1-(triethylsilyl)prop-1-ene

Base Information

• Chemical Name: (E)-3-phenoxy-1-(triethylsilyl)prop-1-ene
• CAS No.: 75476-58-3
• Molecular Formula: C₁₅H₂₄OSi
• Molecular Weight: 248.44
• Mol file: 75476-58-3.mol

Synonyms:(E)-3-phenoxy-1-(triethylsilyl)prop-1-ene

Chemical Property of (E)-3-phenoxy-1-(triethylsilyl)prop-1-ene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (E)-3-phenoxy-1-(triethylsilyl)prop-1-ene

There total 6 articles about (E)-3-phenoxy-1-(triethylsilyl)prop-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

triethylsilane (617-86-7) + 1-phenoxy-2-propyne (13610-02-1) → (E)-3-phenoxy-1-(triethylsilyl)prop-1-ene (75476-58-3)

Guidance literature:

With C₆₀H₈₄Cl₂O₆P₂PtS₂^(2-)*2Na⁽¹⁺⁾; In water; at 60 ℃; for 6h; stereoselective reaction; Inert atmosphere; Green chemistry;

DOI:10.1039/c7gc02823g

Reference yield: 80.0%

triethylsilane (617-86-7) + allyl phenyl ether (1746-13-0) → 1-Phenoxy-3-triethylsilyl-1-propen (75476-59-4) + (E)-3-phenoxy-1-(triethylsilyl)prop-1-ene (75476-58-3)

Guidance literature:

dodecacarbonyl-triangulo-triruthenium; at 50 ℃; for 12h; Yields of byproduct given;

Reference yield:

triethylsilane (617-86-7) + 1-phenoxy-2-propyne (13610-02-1) → (Z)-(3-phenoxyprop-1-ene-1,2-diyl)bis(triethylsilane) (1400817-62-0) + (E)-3-phenoxy-1-(triethylsilyl)prop-1-ene (75476-58-3)

Guidance literature:

With gold nanoparticles on TiO₂; In 1,2-dichloro-ethane; at 70 ℃; for 3h; Overall yield = 83 %; regioselective reaction;

DOI:10.1016/j.tet.2012.08.021

upstream raw materials:

triethylsilane

allyl phenyl ether

1-phenoxy-2-propyne