N-benzyl-2-ethenyl-4-methylaniline

Base Information

Chemical Name:N-benzyl-2-ethenyl-4-methylaniline
CAS No.:809231-07-0
Molecular Formula:C16H17 N
Molecular Weight:223.31288
Hs Code.:
DSSTox Substance ID:DTXSID50460913
Wikidata:Q82285091
Mol file:809231-07-0.mol

Synonyms:809231-07-0;SCHEMBL24928429;DTXSID50460913;AG-H-25415

Suppliers and Price of N-benzyl-2-ethenyl-4-methylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-benzyl-2-ethenyl-4-methylaniline

Chemical Property:

PSA：12.03000
LogP:4.32310
XLogP3:4.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:223.136099547
Heavy Atom Count:17
Complexity:230

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)NCC2=CC=CC=C2)C=C

Technology Process of N-benzyl-2-ethenyl-4-methylaniline

There total 4 articles about N-benzyl-2-ethenyl-4-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 2,4,6-trivinylcyclotriboroxane*pyridine complex

: 809231-03-6
N-benzyl-2-bromo-4-methylbenzeneamine

: 809231-07-0
benzyl(2-vinyl-4-methylphenyl)amine

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; for 20h; Heating;
DOI:10.1021/jo048723e

Reference yield:

2-bromo-p-toluidine: 583-68-6
2-bromo-p-toluidine

: 809231-07-0
benzyl(2-vinyl-4-methylphenyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 4 h

2: 2.32 g / NaBH₄ / methanol / 20 °C

3: 73 percent / K₂CO₃ / Pd(PPh₃)4 / 1,2-dimethoxy-ethane; H₂O / 20 h / Heating

With sodium tetrahydroborate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; 1,2-dimethoxyethane; water; 3: Suzuki-Miyaura reaction;
DOI:10.1021/jo048723e

Reference yield:

: 75767-88-3
(2-Bromo-4-methyl-phenyl)-[1-phenyl-meth-(Z)-ylidene]-amine

: 809231-07-0
benzyl(2-vinyl-4-methylphenyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1: 2.32 g / NaBH₄ / methanol / 20 °C

2: 73 percent / K₂CO₃ / Pd(PPh₃)4 / 1,2-dimethoxy-ethane; H₂O / 20 h / Heating

With sodium tetrahydroborate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; 1,2-dimethoxyethane; water; 2: Suzuki-Miyaura reaction;
DOI:10.1021/jo048723e