C₂₈H₃₂O₃

Base Information

• Chemical Name: C₂₈H₃₂O₃
• CAS No.: 1443230-65-6
• Molecular Formula: C₂₈H₃₂O₃
• Molecular Weight: 416.56
• Mol file: 1443230-65-6.mol

Synonyms:C₂₈H₃₂O₃

Chemical Property of C₂₈H₃₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₃₂O₃

There total 3 articles about C₂₈H₃₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

C30H38O9S2 (1443230-66-7) → C28H32O3 (1443230-65-6)

Guidance literature:

With sodium iodide; zinc; In N,N-dimethyl-formamide; for 4h; Reflux; Inert atmosphere;

DOI:10.1002/ejoc.201201184

Reference yield:

C33H42O9S4 (1443230-64-5) → C28H32O3 (1443230-65-6)

Guidance literature:

Multi-step reaction with 2 steps

1: nickel dichloride; sodium tetrahydroborate / methanol; tetrahydrofuran / 0.5 h / Cooling with ice

2: zinc; sodium iodide / N,N-dimethyl-formamide / 4 h / Reflux; Inert atmosphere

With sodium tetrahydroborate; sodium iodide; nickel dichloride; zinc; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201201184

Reference yield:

C31H38O5S2 (1443230-59-8) → C28H32O3 (1443230-65-6)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 1 h / Cooling with ice

2: nickel dichloride; sodium tetrahydroborate / methanol; tetrahydrofuran / 0.5 h / Cooling with ice

3: zinc; sodium iodide / N,N-dimethyl-formamide / 4 h / Reflux; Inert atmosphere

With sodium tetrahydroborate; triethylamine; sodium iodide; nickel dichloride; zinc; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201201184

upstream raw materials:

C₃₃H₄₂O₉S₄

C₃₀H₃₈O₉S₂

C₃₁H₃₈O₅S₂

Downstream raw materials:

C₄₀H₅₆O₃

(3S,5R)-1-(4-methoxyphenyl)nonadecane-3,5-diol

(3S,5R)-1-(4-hydroxyphenyl)nonadecane-3,5-diol