phenyl 4-O-acetyl-3-O-(t-butyldimethylsilyl)-6-O-benzyl-2-O-(2-methoxyethoxymethyl)-1-seleno-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 4-O-acetyl-3-O-(t-butyldimethylsilyl)-6-O-benzyl-2-O-(2-methoxyethoxymethyl)-1-seleno-β-D-glucopyranoside
CAS No.:1251542-37-6
Molecular Formula:C₃₁H₄₆O₈SeSi
Molecular Weight:653.747
Hs Code.:

Synonyms:phenyl 4-O-acetyl-3-O-(t-butyldimethylsilyl)-6-O-benzyl-2-O-(2-methoxyethoxymethyl)-1-seleno-β-D-glucopyranoside

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Chemical Property of phenyl 4-O-acetyl-3-O-(t-butyldimethylsilyl)-6-O-benzyl-2-O-(2-methoxyethoxymethyl)-1-seleno-β-D-glucopyranoside

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Technology Process of phenyl 4-O-acetyl-3-O-(t-butyldimethylsilyl)-6-O-benzyl-2-O-(2-methoxyethoxymethyl)-1-seleno-β-D-glucopyranoside

There total 1 articles about phenyl 4-O-acetyl-3-O-(t-butyldimethylsilyl)-6-O-benzyl-2-O-(2-methoxyethoxymethyl)-1-seleno-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 1228930-02-6
phenyl 4-O-acetyl-6-O-benzyl-3-O-(tert-butyldimethylsilyl)-1-seleno-β-D-glucopyranoside

: 1251542-37-6
phenyl 4-O-acetyl-3-O-(t-butyldimethylsilyl)-6-O-benzyl-2-O-(2-methoxyethoxymethyl)-1-seleno-β-D-glucopyranoside

Guidance literature:: 2-Methoxyethoxymethyl chloride; With triethylamine; In diethyl ether; Inert atmosphere;

phenyl 4-O-acetyl-6-O-benzyl-3-O-(tert-butyldimethylsilyl)-1-seleno-β-D-glucopyranoside; In acetonitrile; at 80 - 85 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.07.061

Reference yield: 93.0%

: 1251542-37-6
phenyl 4-O-acetyl-3-O-(t-butyldimethylsilyl)-6-O-benzyl-2-O-(2-methoxyethoxymethyl)-1-seleno-β-D-glucopyranoside

: 1251542-38-7
C₂₅H₄₀O₈Si

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; N-ethyl-N,N-diisopropylamine; In 2,2,4-trimethylpentane; dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.07.061