7-tert-Butoxy-2-(2,3-diphenyl-cyclopropyl)-bicyclo[4.4.1]undeca-1⁽¹⁰⁾,2,4,6,8-pentaene

Base Information

• Chemical Name: 7-tert-Butoxy-2-(2,3-diphenyl-cyclopropyl)-bicyclo[4.4.1]undeca-1⁽¹⁰⁾,2,4,6,8-pentaene
• CAS No.: 102050-66-8
• Molecular Formula: C₃₀H₃₀O
• Molecular Weight: 406.568

Synonyms:7-tert-Butoxy-2-(2,3-diphenyl-cyclopropyl)-bicyclo[4.4.1]undeca-1⁽¹⁰⁾,2,4,6,8-pentaene

Chemical Property of 7-tert-Butoxy-2-(2,3-diphenyl-cyclopropyl)-bicyclo[4.4.1]undeca-1⁽¹⁰⁾,2,4,6,8-pentaene

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Technology Process of 7-tert-Butoxy-2-(2,3-diphenyl-cyclopropyl)-bicyclo[4.4.1]undeca-1⁽¹⁰⁾,2,4,6,8-pentaene

There total 5 articles about 7-tert-Butoxy-2-(2,3-diphenyl-cyclopropyl)-bicyclo[4.4.1]undeca-1⁽¹⁰⁾,2,4,6,8-pentaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

7-tert-Butoxy-2-(2-chloro-2,3-diphenyl-cyclopropyl)-bicyclo[4.4.1]undeca-1(10),2,4,6,8-pentaene (102042-36-4) → 7-tert-Butoxy-2-(2,3-diphenyl-cyclopropyl)-bicyclo[4.4.1]undeca-1(10),2,4,6,8-pentaene (102050-66-8)

Guidance literature:

With potassium tert-butylate;

DOI:10.1246/cl.1985.1447

Reference yield:

2-bromo-7-formyl-1,6-methano<10>annulene (102836-19-1) → 7-tert-Butoxy-2-(2,3-diphenyl-cyclopropyl)-bicyclo[4.4.1]undeca-1(10),2,4,6,8-pentaene (102050-66-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 94 percent

2: 1.) Mg

3: 40 percent

4: 80 percent / tBuOK

With potassium tert-butylate; magnesium;

DOI:10.1246/cl.1985.1447

Reference yield:

2-bromo-7-styryl-1,6-methano<10>annulene (102042-34-2,102042-38-6) → 7-tert-Butoxy-2-(2,3-diphenyl-cyclopropyl)-bicyclo[4.4.1]undeca-1(10),2,4,6,8-pentaene (102050-66-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) Mg

2: 40 percent

3: 80 percent / tBuOK

With potassium tert-butylate; magnesium;

DOI:10.1246/cl.1985.1447

upstream raw materials:

7-tert-Butoxy-2-(2-chloro-2,3-diphenyl-cyclopropyl)-bicyclo[4.4.1]undeca-1⁽¹⁰⁾,2,4,6,8-pentaene

2-bromo-7-formyl-1,6-methano<10>annulene

2-bromo-7-styryl-1,6-methano<10>annulene

triphenyl(phenylmethylene)phosphorane

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