tert-butyl [2-(2-fluorophenyl)-1-(hydroxyimino)-2-oxoethyl]sulfonylcarbamate

Base Information

Chemical Name:tert-butyl [2-(2-fluorophenyl)-1-(hydroxyimino)-2-oxoethyl]sulfonylcarbamate
CAS No.:1447236-97-6
Molecular Formula:C₁₃H₁₅FN₂O₆S
Molecular Weight:346.336
Hs Code.:

Synonyms:tert-butyl [2-(2-fluorophenyl)-1-(hydroxyimino)-2-oxoethyl]sulfonylcarbamate

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Chemical Property of tert-butyl [2-(2-fluorophenyl)-1-(hydroxyimino)-2-oxoethyl]sulfonylcarbamate

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Technology Process of tert-butyl [2-(2-fluorophenyl)-1-(hydroxyimino)-2-oxoethyl]sulfonylcarbamate

There total 3 articles about tert-butyl [2-(2-fluorophenyl)-1-(hydroxyimino)-2-oxoethyl]sulfonylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1447236-83-0
tert-butyl [2-(2-fluorophenyl)-2-oxoethyl]sulfonylcarbamate

: 1447236-97-6
tert-butyl [2-(2-fluorophenyl)-1-(hydroxyimino)-2-oxoethyl]sulfonylcarbamate

Guidance literature:: With sodium nitrite; In tetrahydrofuran; water; acetic acid; at 0 ℃; for 19h; Inert atmosphere;
DOI:10.1021/jo400976f

Reference yield:

: 147751-16-4
tert-butyl (methylsulfonyl)carbamate

: 1447236-97-6
tert-butyl [2-(2-fluorophenyl)-1-(hydroxyimino)-2-oxoethyl]sulfonylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; diisopropylamine / hexane; tetrahydrofuran-d8 / 1 h / 0 °C / Inert atmosphere

1.2: 1.5 h / 0 °C / Inert atmosphere

2.1: sodium nitrite / tetrahydrofuran; water; acetic acid / 19 h / 0 °C / Inert atmosphere

With n-butyllithium; diisopropylamine; sodium nitrite; In tetrahydrofuran; tetrahydrofuran-d8; hexane; water; acetic acid;
DOI:10.1021/jo400976f

Reference yield:

: 394-35-4
methyl 2-fluorobenzoate

: 1447236-97-6
tert-butyl [2-(2-fluorophenyl)-1-(hydroxyimino)-2-oxoethyl]sulfonylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; diisopropylamine / hexane; tetrahydrofuran-d8 / 1 h / 0 °C / Inert atmosphere

1.2: 1.5 h / 0 °C / Inert atmosphere

2.1: sodium nitrite / tetrahydrofuran; water; acetic acid / 19 h / 0 °C / Inert atmosphere

With n-butyllithium; diisopropylamine; sodium nitrite; In tetrahydrofuran; tetrahydrofuran-d8; hexane; water; acetic acid;
DOI:10.1021/jo400976f