(S,E)-N-(6-((tert-butyldimethylsilyl)oxy)hexylidene)-2,4,6-trimethylbenzenesulfinamide

Base Information

Chemical Name:(S,E)-N-(6-((tert-butyldimethylsilyl)oxy)hexylidene)-2,4,6-trimethylbenzenesulfinamide
CAS No.:1279697-22-1
Molecular Formula:C₂₁H₃₇NO₂SSi
Molecular Weight:395.682
Hs Code.:

Synonyms:(S,E)-N-(6-((tert-butyldimethylsilyl)oxy)hexylidene)-2,4,6-trimethylbenzenesulfinamide

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Chemical Property of (S,E)-N-(6-((tert-butyldimethylsilyl)oxy)hexylidene)-2,4,6-trimethylbenzenesulfinamide

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Technology Process of (S,E)-N-(6-((tert-butyldimethylsilyl)oxy)hexylidene)-2,4,6-trimethylbenzenesulfinamide

There total 1 articles about (S,E)-N-(6-((tert-butyldimethylsilyl)oxy)hexylidene)-2,4,6-trimethylbenzenesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1279696-96-6
(2R,4S)-3-[(4-methylphenyl)sulfonyl]-4-(phenylmethyl)-1,2,3-oxathiazolidine 2-oxide

: 118794-69-7
6-[(tert-butyldimethylsilyl)oxy]hexanal

: 2633-66-1
2-mesitylmagnesium bromide

: 1279697-22-1
(S,E)-N-(6-((tert-butyldimethylsilyl)oxy)hexylidene)-2,4,6-trimethylbenzenesulfinamide

Guidance literature:: (2R,4S)-3-[(4-methylphenyl)sulfonyl]-4-(phenylmethyl)-1,2,3-oxathiazolidine 2-oxide; 2-mesitylmagnesium bromide; In tetrahydrofuran; at -68 ℃; Inert atmosphere; Cooling with acetone-dry ice;

With lithium hexamethyldisilazane; In tetrahydrofuran; at -68 - 20 ℃; Inert atmosphere;

6-[(tert-butyldimethylsilyl)oxy]hexanal; With titanium(IV) tetraethanolate; In tetrahydrofuran; at 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.201003222