1-(1'-methoxycarbonyloxybenzyl)-3,5,5-trimethylcyclohex-2-enecarboxaldehyde

Base Information

Chemical Name:1-(1'-methoxycarbonyloxybenzyl)-3,5,5-trimethylcyclohex-2-enecarboxaldehyde
CAS No.:343815-82-7
Molecular Formula:C₁₉H₂₄O₄
Molecular Weight:316.397
Hs Code.:

Synonyms:1-(1'-methoxycarbonyloxybenzyl)-3,5,5-trimethylcyclohex-2-enecarboxaldehyde

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Chemical Property of 1-(1'-methoxycarbonyloxybenzyl)-3,5,5-trimethylcyclohex-2-enecarboxaldehyde

Chemical Property:

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Technology Process of 1-(1'-methoxycarbonyloxybenzyl)-3,5,5-trimethylcyclohex-2-enecarboxaldehyde

There total 3 articles about 1-(1'-methoxycarbonyloxybenzyl)-3,5,5-trimethylcyclohex-2-enecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78-59-1
3,5,5-Trimethylcyclohex-2-en-1-one

: 343815-82-7
1-(1'-methoxycarbonyloxybenzyl)-3,5,5-trimethylcyclohex-2-enecarboxaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-butyllithium / 1) THF, -78 deg C, 1 h; 2) THF, reflux, 2 h

2: 1.) n-butyllithium / 1) THF, hexane, -78 deg C, 1 h; 2) 30 min, THF

3: tetrahydrofuran / 1) -78 deg C, 1 h; 2) -78 deg C --> room temperature, 2 - 3 h

With n-butyllithium; In tetrahydrofuran;
DOI:10.1021/ja00538a027

Reference yield:

: 343221-98-7
[1-Phenyl-meth-(Z)-ylidene]-[3,5,5-trimethyl-cyclohex-2-en-(Z)-ylidenemethyl]-amine

: 343815-82-7
1-(1'-methoxycarbonyloxybenzyl)-3,5,5-trimethylcyclohex-2-enecarboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1) THF, hexane, -78 deg C, 1 h; 2) 30 min, THF

2: tetrahydrofuran / 1) -78 deg C, 1 h; 2) -78 deg C --> room temperature, 2 - 3 h

With n-butyllithium; In tetrahydrofuran;
DOI:10.1021/ja00538a027