Technology Process of 1-phenylindane-4,7-quinone
There total 5 articles about 1-phenylindane-4,7-quinone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium sulfate; silver(l) oxide;
In
benzene;
for 0.75h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 72 percent / conc HCl / pyridine / 1.5 h / 165 - 170 °C
2: 2.) sodium sulfate, silver oxide / 1.) THf, ether, -75 deg C, 15 min, r.t., 45 min, 2.) r.t., 1 h
3: 77 percent / H2 / 10percent Pd/C / ethanol / 0.25 h
4: 97 percent / sodium sulfate, silver oxide / benzene / 0.75 h / Ambient temperature
With
hydrogenchloride; hydrogen; sodium sulfate; silver(l) oxide;
palladium on activated charcoal;
In
pyridine; ethanol; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 83 percent / AlCl3 / 1,2-dichloro-ethane / 2 h / Ambient temperature
2: 72 percent / conc HCl / pyridine / 1.5 h / 165 - 170 °C
3: 2.) sodium sulfate, silver oxide / 1.) THf, ether, -75 deg C, 15 min, r.t., 45 min, 2.) r.t., 1 h
4: 77 percent / H2 / 10percent Pd/C / ethanol / 0.25 h
5: 97 percent / sodium sulfate, silver oxide / benzene / 0.75 h / Ambient temperature
With
hydrogenchloride; aluminium trichloride; hydrogen; sodium sulfate; silver(l) oxide;
palladium on activated charcoal;
In
pyridine; ethanol; 1,2-dichloro-ethane; benzene;
