diethyl N,N'-<4-(10-undecenyloxy)-2,6-pyridinediyl>bis

Base Information

Chemical Name:diethyl N,N'-<4-(10-undecenyloxy)-2,6-pyridinediyl>bis
CAS No.:101631-01-0
Molecular Formula:C₂₂H₃₅N₃O₅
Molecular Weight:421.537
Hs Code.:

diethyl N,N'-<4-(10-undecenyloxy)-2,6-pyridinediyl>bis<carbamate>

Synonyms:diethyl N,N'-<4-(10-undecenyloxy)-2,6-pyridinediyl>bis

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Chemical Property of diethyl N,N'-<4-(10-undecenyloxy)-2,6-pyridinediyl>bis

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Technology Process of diethyl N,N'-<4-(10-undecenyloxy)-2,6-pyridinediyl>bis

There total 1 articles about diethyl N,N'-<4-(10-undecenyloxy)-2,6-pyridinediyl>bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7766-50-9
1-undecen-11-ylbromide

: 101631-01-0
diethyl N,N'-<4-(10-undecenyloxy)-2,6-pyridinediyl>bis

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Na / 2.) 18-crown-6 / 1.) butanol; 2.) toluene, reflux, overnight

2: 65 percent / H₂NNH₂ / by Markees et al.

3: 9percent HCl, NaNO₂ / H₂O / 2 h / 10 - 15 °C

4: 5 h / Heating

With hydrogenchloride; sodium; hydrazine; sodium nitrite; 18-crown-6 ether; In water;
DOI:10.1021/ja00272a027

Reference yield:

: 101631-01-0
diethyl N,N'-<4-(10-undecenyloxy)-2,6-pyridinediyl>bis

: 101631-04-3
N,N'-<4-(11-(dimethylchlorosilyl)undecyloxy)-2,6-pyridinediyl>bis<2-(S)-phenylbutanamide>

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / KOH / ethanol / 3 h / Heating

2: 25 percent / N-methylmorpholine / CHCl₃ / -20 - -15 °C

3: platinic acid / 2 h / Heating

With 4-methyl-morpholine; potassium hydroxide; platinic acid; In ethanol; chloroform;
DOI:10.1021/ja00272a027

Reference yield:

: 101631-01-0
diethyl N,N'-<4-(10-undecenyloxy)-2,6-pyridinediyl>bis

: <4-(undecyloxy)-2,6-pyridinediyl>bis<(S)-2-phenylbutanamide>

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / KOH / ethanol / 3 h / Heating

2: N-methylmorpholine / CHCl₃ / -20 - -15 °C

With 4-methyl-morpholine; potassium hydroxide; In ethanol; chloroform;
DOI:10.1021/ja00272a027