Cyclobutaneethanol, 2,2-dimethyl-3-(1-methylethenyl)-, propanoate, (1R,3S)- (9CI)

Base Information

Chemical Name:Cyclobutaneethanol, 2,2-dimethyl-3-(1-methylethenyl)-, propanoate, (1R,3S)- (9CI)
CAS No.:808229-87-0
Molecular Formula:C₁₄H₂₄O₂
Molecular Weight:224.343
Hs Code.:
Mol file:808229-87-0.mol

Synonyms:Cyclobutaneethanol,2,2-dimethyl-3-(1-methylethenyl)-, propanoate, (1R,3S)- (9CI)

Suppliers and Price of Cyclobutaneethanol, 2,2-dimethyl-3-(1-methylethenyl)-, propanoate, (1R,3S)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclobutaneethanol, 2,2-dimethyl-3-(1-methylethenyl)-, propanoate, (1R,3S)- (9CI)

Chemical Property:

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Technology Process of Cyclobutaneethanol, 2,2-dimethyl-3-(1-methylethenyl)-, propanoate, (1R,3S)- (9CI)

There total 2 articles about Cyclobutaneethanol, 2,2-dimethyl-3-(1-methylethenyl)-, propanoate, (1R,3S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82467-65-0
(+)-2-<(1S,3R)-3-Acetyl-2,2-dimethylcyclobutyl>ethanol

: 808229-87-0
(+)-cis-(1R)-3-isopropenyl-2,2-dimethylcyclobutaneethanol propionate

Guidance literature:: Multi-step reaction with 2 steps

1: 41.6 percent / xylidene / diethyl ether / Ambient temperature

2: 1.) NaH / 1.) DMSO, 60 deg C, 2 h, 2.) DMSO, from 60 deg C to 70 deg C, 5 h

With xylidene; sodium hydride; In diethyl ether;
DOI:10.1080/00397919508011458

Reference yield:

: 2065-66-9
methyl-triphenylphosphonium iodide

: (+)-cis-(1R)-2,2-dimethyl-3-acetylcyclobutaneethanol propionate

: 808229-87-0
(+)-cis-(1R)-3-isopropenyl-2,2-dimethylcyclobutaneethanol propionate

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMSO, 60 deg C, 2 h, 2.) DMSO, from 60 deg C to 70 deg C, 5 h;
DOI:10.1080/00397919508011458