N-cyclohexyl-N'-pentylsulfamide

Base Information

• Chemical Name: N-cyclohexyl-N'-pentylsulfamide
• CAS No.: 85515-62-4
• Molecular Formula: C₁₁H₂₄N₂O₂S
• Molecular Weight: 248.39
• Mol file: 85515-62-4.mol

Synonyms:N-cyclohexyl-N'-pentylsulfamide

Chemical Property of N-cyclohexyl-N'-pentylsulfamide

Chemical Property:

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Technology Process of N-cyclohexyl-N'-pentylsulfamide

There total 1 articles about N-cyclohexyl-N'-pentylsulfamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

triethylammonium N-cyclohexylsulfamate + n-Pentylamine (110-58-7) → N-cyclohexyl-N'-pentylsulfamide (85515-62-4)

Guidance literature:

triethylammonium N-cyclohexylsulfamate; With trifluoromethylsulfonic anhydride; Triphenylphosphine oxide; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 ℃; for 0.25h; Inert atmosphere;

n-Pentylamine; In dichloromethane; at -78 - 22 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2019.02.063

upstream raw materials:

n-Pentylamine