Technology Process of C35H64O6Si2
There total 15 articles about C35H64O6Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; water;
at 0 ℃;
DOI:10.1246/cl.2007.278
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 100 percent / TEA; DMAP / CH2Cl2
2: 94 percent / AcOH; H2O / tetrahydrofuran / 50 °C
3: 98 percent / K2CO3 / methanol; CH2Cl2
4: 99 percent / MeI; NaHCO3 / H2O; acetone / 40 °C
5: 99 percent / H2; quinoline / Lindlar cat. / ethyl acetate
6: 65 percent / Eu(fod)3 / xylene / 120 °C
7: 99 percent / AgNO3; pyridine / acetonitrile
8: 94 percent / MCPBA; NaHCO3 / CH2Cl2; H2O / 0 °C
With
pyridine; quinoline; dmap; TEA; water; hydrogen; sodium hydrogencarbonate; potassium carbonate; silver nitrate; acetic acid; 3-chloro-benzenecarboperoxoic acid; Eu(fod)3; methyl iodide;
Lindlar catalyst;
In
tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; acetonitrile; xylene;
DOI:10.1246/cl.2007.278
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 98 percent / K2CO3 / methanol; CH2Cl2
2: 99 percent / MeI; NaHCO3 / H2O; acetone / 40 °C
3: 99 percent / H2; quinoline / Lindlar cat. / ethyl acetate
4: 65 percent / Eu(fod)3 / xylene / 120 °C
5: 99 percent / AgNO3; pyridine / acetonitrile
6: 94 percent / MCPBA; NaHCO3 / CH2Cl2; H2O / 0 °C
With
pyridine; quinoline; hydrogen; sodium hydrogencarbonate; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; Eu(fod)3; methyl iodide;
Lindlar catalyst;
In
methanol; dichloromethane; water; ethyl acetate; acetone; acetonitrile; xylene;
DOI:10.1246/cl.2007.278