Diethyl-{2-[1-(3-methyl-pyridin-2-yl)-1H-imidazol-2-ylsulfanylmethyl]-phenyl}-amine

Base Information

Chemical Name:Diethyl-{2-[1-(3-methyl-pyridin-2-yl)-1H-imidazol-2-ylsulfanylmethyl]-phenyl}-amine
CAS No.:117348-31-9
Molecular Formula:C₂₀H₂₄N₄S
Molecular Weight:352.503
Hs Code.:

Synonyms:Diethyl-{2-[1-(3-methyl-pyridin-2-yl)-1H-imidazol-2-ylsulfanylmethyl]-phenyl}-amine

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Chemical Property of Diethyl-{2-[1-(3-methyl-pyridin-2-yl)-1H-imidazol-2-ylsulfanylmethyl]-phenyl}-amine

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Technology Process of Diethyl-{2-[1-(3-methyl-pyridin-2-yl)-1H-imidazol-2-ylsulfanylmethyl]-phenyl}-amine

There total 6 articles about Diethyl-{2-[1-(3-methyl-pyridin-2-yl)-1H-imidazol-2-ylsulfanylmethyl]-phenyl}-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113805-35-9
(2-Chloromethyl-phenyl)-diethyl-amine

: 117296-72-7
2-mercapto-1-<2-(3-methylpyridyl)>imidazole

: 117348-31-9
Diethyl-{2-[1-(3-methyl-pyridin-2-yl)-1H-imidazol-2-ylsulfanylmethyl]-phenyl}-amine

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; at 0 ℃; for 3h;
DOI:10.1021/jm950610n

Reference yield:

: 1603-40-3
3-methylpyridin-2-ylamine

: 117348-31-9
Diethyl-{2-[1-(3-methyl-pyridin-2-yl)-1H-imidazol-2-ylsulfanylmethyl]-phenyl}-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / toluene / 18 h / Heating

2: 63 percent / AcOH, HCl / 18 h / Heating

3: NaOH / dimethylformamide / 3 h / 0 °C

With hydrogenchloride; sodium hydroxide; acetic acid; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm950610n

Reference yield:

: 394-35-4
methyl 2-fluorobenzoate

: 117348-31-9
Diethyl-{2-[1-(3-methyl-pyridin-2-yl)-1H-imidazol-2-ylsulfanylmethyl]-phenyl}-amine

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / dimethylformamide / Ambient temperature

2: LiAlH₄ / tetrahydrofuran

3: SOCl₂ / CHCl₃

4: NaOH / dimethylformamide / 3 h / 0 °C

With sodium hydroxide; lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm950610n