{Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}⁽¹⁺⁾*BF₄^(1-)*CH₂Cl₂={Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}BF₄*CH₂Cl₂

Base Information

• Chemical Name: {Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}⁽¹⁺⁾*BF₄^(1-)*CH₂Cl₂={Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}BF₄*CH₂Cl₂
• CAS No.: 143890-22-6
• Molecular Formula: BF₄*CH₂Cl₂*C₃₈H₃₂Cl₂CuN₂O₄P₂Rh₂
• Molecular Weight: 1154.63

Synonyms:{Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}⁽¹⁺⁾*BF₄^(1-)*CH₂Cl₂={Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}BF₄*CH₂Cl₂

Chemical Property of {Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}⁽¹⁺⁾*BF₄^(1-)*CH₂Cl₂={Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}BF₄*CH₂Cl₂

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Technology Process of {Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}⁽¹⁺⁾*BF₄^(1-)*CH₂Cl₂={Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}BF₄*CH₂Cl₂

There total 2 articles about {Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}⁽¹⁺⁾*BF₄^(1-)*CH₂Cl₂={Rh₂Cu(CO)2(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl₂}BF₄*CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

tetrakis(acetonitrile)copper(I)tetrafluoroborate + {Rh(CO)(C5H3N(P(C6H5)2)(OCH3))2Cl} (143890-19-1) → {Rh2Cu(CO)2(C5H3N(P(C6H5)2)(OCH3))2Cl2}(1+)*BF4(1-)*CH2Cl2={Rh2Cu(CO)2(C5H3N(P(C6H5)2)(OCH3))2Cl2}BF4*CH2Cl2 (143890-22-6)

Guidance literature:

With CH₂Cl₂; In dichloromethane; (N2); addn. of solid Cu-complex to a stirred soln. of the Rh-complex in CH2Cl2, stirring for 15 min; the volume of the soln. is reduced, addn. of diethyl ether, filtration of the ppt., washing (diethyl ether), drying in vac., elem. anal.;

Reference yield:

tetrakis(acetonitrile)copper(I)tetrafluoroborate + {Rh(CO)(C5H3N(P(C6H5)2)(OCH3))Cl}2 (143890-23-7) → {Rh2Cu(CO)2(C5H3N(P(C6H5)2)(OCH3))2Cl2}(1+)*BF4(1-)*CH2Cl2={Rh2Cu(CO)2(C5H3N(P(C6H5)2)(OCH3))2Cl2}BF4*CH2Cl2 (143890-22-6)

Guidance literature:

With CH₂Cl₂; In dichloromethane; (N2); addn. of solid Cu-complex to a stirred soln. of the Rh-complex in CH2Cl2, stirring for 20 min; the volume of the soln. is reduced, addn. of diethyl ether, filtration of the ppt., washing (diethyl ether), drying in vac.;

upstream raw materials:

{Rh(CO)(C₅H₃N(P(C₆H₅)2)(OCH₃))Cl}2

{Rh(CO)(C₅H₃N(P(C₆H₅)2)(OCH₃))2Cl}

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