2'-O-[1-(4-Chlorophenyl)-4-ethoxypiperidin-4-yl]-6-N-pivaloyladenosine

Base Information

Chemical Name:2'-O-[1-(4-Chlorophenyl)-4-ethoxypiperidin-4-yl]-6-N-pivaloyladenosine
CAS No.:263008-98-6
Molecular Formula:C₂₈H₃₇ClN₆O₆
Molecular Weight:589.091
Hs Code.:

Synonyms:2'-O-[1-(4-Chlorophenyl)-4-ethoxypiperidin-4-yl]-6-N-pivaloyladenosine

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Chemical Property of 2'-O-[1-(4-Chlorophenyl)-4-ethoxypiperidin-4-yl]-6-N-pivaloyladenosine

Chemical Property:

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Technology Process of 2'-O-[1-(4-Chlorophenyl)-4-ethoxypiperidin-4-yl]-6-N-pivaloyladenosine

There total 10 articles about 2'-O-[1-(4-Chlorophenyl)-4-ethoxypiperidin-4-yl]-6-N-pivaloyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 908140-97-6
N-(9-{(2R,3R,3aR,9aR)-3-[1-(4-Chloro-phenyl)-4-ethoxy-piperidin-4-yloxy]-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl}-9H-purin-6-yl)-2,2-dimethyl-propionamide

: 263008-98-6
2'-O-[1-(4-Chlorophenyl)-4-ethoxypiperidin-4-yl]-6-N-pivaloyladenosine

Guidance literature:: With tetraethylammonium fluoride; In tetrahydrofuran;
DOI:10.1081/NCN-200060150

Reference yield:

: 263008-89-5
1-(4-Chlorophenyl)-4,4-diethoxypiperidine

: 263008-98-6
2'-O-[1-(4-Chlorophenyl)-4-ethoxypiperidin-4-yl]-6-N-pivaloyladenosine

Guidance literature:: Multi-step reaction with 3 steps

1: Huenig's base; BF₃*Et₂O / CH₂Cl₂ / 0 °C

2: DCA / CH₂Cl₂

3: TEAF / tetrahydrofuran

With dichloro-acetic acid; boron trifluoride diethyl etherate; tetraethylammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1081/NCN-200060150

Reference yield:

: 263008-90-8
1-(4-Chlorophenyl)-4-ethoxy-1,2,5,6-tetrahydropyridine

: 263008-98-6
2'-O-[1-(4-Chlorophenyl)-4-ethoxypiperidin-4-yl]-6-N-pivaloyladenosine

Guidance literature:: Multi-step reaction with 2 steps

1: DCA / CH₂Cl₂

2: TEAF / tetrahydrofuran

With dichloro-acetic acid; tetraethylammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1081/NCN-200060150