(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tetrahydro-furan-3-yl ester

Base Information

Chemical Name:(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tetrahydro-furan-3-yl ester
CAS No.:1026246-70-7
Molecular Formula:C₂₁H₂₄N₄O₃
Molecular Weight:380.447
Hs Code.:

Synonyms:(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tetrahydro-furan-3-yl ester

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Chemical Property of (2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tetrahydro-furan-3-yl ester

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Technology Process of (2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tetrahydro-furan-3-yl ester

There total 7 articles about (2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 922723-30-6
2-azido-1-benzyl-3-phenyl-propylamine

: 160333-50-6
1-({[(3R)-tetrahydrofuran-3-yloxy]carbonyl}oxy)pyrrolidine-2,5-dione

: 1026246-70-7
(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tetrahydro-furan-3-yl ester

Guidance literature:: With triethanolamine; In water; toluene; at 20 ℃; for 1h;
DOI:10.1021/jm060754+

Reference yield:

: 6921-34-2
benzylmagnesium chloride

: 1026246-70-7
(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: CuBr*DMS / tetrahydrofuran / 0.17 h / -78 °C

1.2: tetrahydrofuran / -78 - 20 °C

2.1: 91 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

3.1: 64 percent / NaN₃ / dimethylformamide / 16 h / 60 °C

4.1: trifluoroacetic acid / CH₂Cl₂ / 0.5 h / 0 °C

5.1: triethanolamine / toluene; H₂O / 1 h / 20 °C

With sodium azide; copper(I) bromide dimethylsulfide complex; triethanolamine; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm060754+

Reference yield:

: 922722-32-5
(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tert-butyl ester

: 1026246-70-7
(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / CH₂Cl₂ / 0.5 h / 0 °C

2: triethanolamine / toluene; H₂O / 1 h / 20 °C

With triethanolamine; trifluoroacetic acid; In dichloromethane; water; toluene;
DOI:10.1021/jm060754+