(E)-1-chloro-4-(5,5,5-trifluoro-4-(phenylsulfonyl)pent-1-enyl)benzene

Base Information

Chemical Name:(E)-1-chloro-4-(5,5,5-trifluoro-4-(phenylsulfonyl)pent-1-enyl)benzene
CAS No.:1414925-92-0
Molecular Formula:C₁₇H₁₄ClF₃O₂S
Molecular Weight:374.811
Hs Code.:

Synonyms:(E)-1-chloro-4-(5,5,5-trifluoro-4-(phenylsulfonyl)pent-1-enyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-chloro-4-(5,5,5-trifluoro-4-(phenylsulfonyl)pent-1-enyl)benzene

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Technology Process of (E)-1-chloro-4-(5,5,5-trifluoro-4-(phenylsulfonyl)pent-1-enyl)benzene

There total 3 articles about (E)-1-chloro-4-(5,5,5-trifluoro-4-(phenylsulfonyl)pent-1-enyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1233720-26-7
(E)-3-(4-chlorophenyl)allyl ethyl carbonate

: 56354-44-0
β,β,β-trifluoroethyl phenyl sulfone

: 1414925-92-0
(E)-1-chloro-4-(5,5,5-trifluoro-4-(phenylsulfonyl)pent-1-enyl)benzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 60 ℃; for 22h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.09.094

Reference yield:

: 108-98-5
thiophenol

: 1414925-92-0
(E)-1-chloro-4-(5,5,5-trifluoro-4-(phenylsulfonyl)pent-1-enyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / mineral oil; N,N-dimethyl-formamide

2: dihydrogen peroxide / acetic acid / 3 h / 100 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 22 h / 60 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; sodium hydride; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tetlet.2012.09.094

Reference yield:

: 2262-07-9
2,2,2-trifluoroethyl phenyl sulfide

: 1414925-92-0
(E)-1-chloro-4-(5,5,5-trifluoro-4-(phenylsulfonyl)pent-1-enyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide / acetic acid / 3 h / 100 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 22 h / 60 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; In tetrahydrofuran; acetic acid;
DOI:10.1016/j.tetlet.2012.09.094