2-[(3R)-3-(tert-butyl-dimethyl-silanyloxymethyl)-2-oxo-5-phenyl-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-N-[(2R,3S)-2-tertbutylthio-5-oxo-tetrahydrofuran-3-yl]-acetamide

Base Information

Chemical Name:2-[(3R)-3-(tert-butyl-dimethyl-silanyloxymethyl)-2-oxo-5-phenyl-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-N-[(2R,3S)-2-tertbutylthio-5-oxo-tetrahydrofuran-3-yl]-acetamide
CAS No.:1234549-25-7
Molecular Formula:C₃₂H₄₃N₃O₅SSi
Molecular Weight:609.862
Hs Code.:

2-[(3R)-3-(tert-butyl-dimethyl-silanyloxymethyl)-2-oxo-5-phenyl-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-N-[(2R,3S)-2-tertbutylthio-5-oxo-tetrahydrofuran-3-yl]-acetamide

Synonyms:2-[(3R)-3-(tert-butyl-dimethyl-silanyloxymethyl)-2-oxo-5-phenyl-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-N-[(2R,3S)-2-tertbutylthio-5-oxo-tetrahydrofuran-3-yl]-acetamide

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Chemical Property of 2-[(3R)-3-(tert-butyl-dimethyl-silanyloxymethyl)-2-oxo-5-phenyl-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-N-[(2R,3S)-2-tertbutylthio-5-oxo-tetrahydrofuran-3-yl]-acetamide

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Technology Process of 2-[(3R)-3-(tert-butyl-dimethyl-silanyloxymethyl)-2-oxo-5-phenyl-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-N-[(2R,3S)-2-tertbutylthio-5-oxo-tetrahydrofuran-3-yl]-acetamide

There total 1 articles about 2-[(3R)-3-(tert-butyl-dimethyl-silanyloxymethyl)-2-oxo-5-phenyl-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-N-[(2R,3S)-2-tertbutylthio-5-oxo-tetrahydrofuran-3-yl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 896746-87-5
[(3R)-3-({[tert-butyl(dimethyl)silyl]oxy}methyl)-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-1-yl]acetic acid

: C₈H₁₅NO₂S

: 1234549-25-7
2-[(3R)-3-(tert-butyl-dimethyl-silanyloxymethyl)-2-oxo-5-phenyl-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-N-[(2R,3S)-2-tertbutylthio-5-oxo-tetrahydrofuran-3-yl]-acetamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 15h;
DOI:10.1016/j.ejmech.2010.04.003

Reference yield: 82.0%

: 1234549-25-7
2-[(3R)-3-(tert-butyl-dimethyl-silanyloxymethyl)-2-oxo-5-phenyl-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-N-[(2R,3S)-2-tertbutylthio-5-oxo-tetrahydrofuran-3-yl]-acetamide

: 1234549-28-0
N-[(2R,3S)-2-tert-butylthio-5-oxo-tetrahydrofuran-3-yl]-2-[(3R)-3-hydroxy methyl-2-oxo-5-phenyl-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-acetamide

Guidance literature:: 2-[(3R)-3-(tert-butyl-dimethyl-silanyloxymethyl)-2-oxo-5-phenyl-2,3-dihydro-benzo[e][1,4]diazepin-1-yl]-N-[(2R,3S)-2-tertbutylthio-5-oxo-tetrahydrofuran-3-yl]-acetamide; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 5h;

With water; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.ejmech.2010.04.003