13,17-Diethyl-3,7-bis(2-methoxycarbonylethyl)-2,8,12,18-tetramethylporphyrin

Base Information

Chemical Name:13,17-Diethyl-3,7-bis(2-methoxycarbonylethyl)-2,8,12,18-tetramethylporphyrin
CAS No.:992-32-5
Molecular Formula:C₃₆H₄₂N₄O₄
Molecular Weight:594.754
Hs Code.:

Synonyms:13,17-Diethyl-3,7-bis(2-methoxycarbonylethyl)-2,8,12,18-tetramethylporphyrin

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Chemical Property of 13,17-Diethyl-3,7-bis(2-methoxycarbonylethyl)-2,8,12,18-tetramethylporphyrin

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Technology Process of 13,17-Diethyl-3,7-bis(2-methoxycarbonylethyl)-2,8,12,18-tetramethylporphyrin

There total 3 articles about 13,17-Diethyl-3,7-bis(2-methoxycarbonylethyl)-2,8,12,18-tetramethylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 7670-41-9
3,3'-diethyl-4,4'-dimethyldipyrromethane-5,5'-dicarboxylic acid

: 4792-10-3
3-{5-Formyl-2-[5-formyl-3-(2-methoxycarbonyl-ethyl)-4-methyl-1H-pyrrol-2-ylmethyl]-4-methyl-1H-pyrrol-3-yl}-propionic acid methyl ester

: 992-32-5
13,17-diethyl-3,7-bis(2-methoxycarbonylethyl)-2,8,12,18-tetramethylporphyrin

Guidance literature:: 3,3'-diethyl-4,4'-dimethyldipyrromethane-5,5'-dicarboxylic acid; 3-{5-Formyl-2-[5-formyl-3-(2-methoxycarbonyl-ethyl)-4-methyl-1H-pyrrol-2-ylmethyl]-4-methyl-1H-pyrrol-3-yl}-propionic acid methyl ester; With toluene-4-sulfonic acid; In methanol; dichloromethane; at 20 ℃; for 24h;

With zinc diacetate; In methanol; dichloromethane; at 20 ℃; for 72h;

With sulfuric acid; In methanol; for 16h; Further stages.;
DOI:10.1055/s-2008-1032203

Reference yield:

: 7670-41-9
3,3'-diethyl-4,4'-dimethyldipyrromethane-5,5'-dicarboxylic acid

: 4792-10-3
3-{5-Formyl-2-[5-formyl-3-(2-methoxycarbonyl-ethyl)-4-methyl-1H-pyrrol-2-ylmethyl]-4-methyl-1H-pyrrol-3-yl}-propionic acid methyl ester

: 992-32-5
13,17-Diethyl-3,7-bis(2-methoxycarbonylethyl)-2,8,12,18-tetramethylporphyrin

Guidance literature:: With zinc diacetate; toluene-4-sulfonic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂, MeOH, overnight, 2.) MeOH, 12 h;
DOI:10.1021/jo960720h

Reference yield:

: C₁₈H₂₄N₂O₅

: 4792-10-3
3-{5-Formyl-2-[5-formyl-3-(2-methoxycarbonyl-ethyl)-4-methyl-1H-pyrrol-2-ylmethyl]-4-methyl-1H-pyrrol-3-yl}-propionic acid methyl ester

: 992-32-5
13,17-Diethyl-3,7-bis(2-methoxycarbonylethyl)-2,8,12,18-tetramethylporphyrin

Guidance literature:: With toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; Yield given. Multistep reaction; 1.) CH₂Cl₂, MeOH, r.t., 24 h, 2.) CH₂Cl₂, 1 h;