4,4-diphenylcyclohexyl dichlorophosphite

Base Information

• Chemical Name: 4,4-diphenylcyclohexyl dichlorophosphite
• CAS No.: 214695-72-4
• Molecular Formula: C₁₈H₁₉Cl₂OP
• Molecular Weight: 353.228
• Mol file: 214695-72-4.mol

Synonyms:4,4-diphenylcyclohexyl dichlorophosphite

Chemical Property of 4,4-diphenylcyclohexyl dichlorophosphite

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4,4-diphenylcyclohexyl dichlorophosphite

There total 1 articles about 4,4-diphenylcyclohexyl dichlorophosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4-diphenyl-cyclohexanol (42420-85-9) → 4,4-diphenylcyclohexyl dichlorophosphite (214695-72-4)

Guidance literature:

With phosphorus trichloride; In tetrahydrofuran; at -5 - 0 ℃; for 0.5h;

DOI:10.1002/chem.200500338

Reference yield:

1H-imidazole (288-32-4) + 4,4-diphenylcyclohexyl dichlorophosphite (214695-72-4) → C21H22ClN2OP

Guidance literature:

In tetrahydrofuran; at -6 - 0 ℃; for 0.5h;

DOI:10.1021/ja017168k

Reference yield:

{[2-(bis-tert-butoxycarbonylmethyl-amino)-ethyl]-[2-(tert-butoxycarbonylmethyl-methyl-amino)-3-hydroxy-propyl]-amino}-acetic acid tert-butyl ester + 4,4-diphenylcyclohexyl dichlorophosphite (214695-72-4) → ({1-({[2-(bis-tert-butoxycarbonylmethyl-amino)-ethyl]-tert-butoxycarbonylmethyl-amino}-methyl)-2-[(4,4-diphenyl-cyclohexyloxy)-hydroxy-phosphanyloxy]-ethyl}-methyl-amino)-acetic acid tert-butyl ester

Guidance literature:

4,4-diphenylcyclohexyl dichlorophosphite; With 1H-imidazole; In tetrahydrofuran; at 0 - 5 ℃; for 0.333333h;

{[2-(bis-tert-butoxycarbonylmethyl-amino)-ethyl]-[2-(tert-butoxycarbonylmethyl-methyl-amino)-3-hydroxy-propyl]-amino}-acetic acid tert-butyl ester; In tetrahydrofuran; hexane; at -5 - 0 ℃; for 0.333333h;

DOI:10.1002/chem.200500338

upstream raw materials:

4,4-diphenyl-cyclohexanol