4b-hydroxy-4b,5,6,7,8,9-hexahydro-10-oxa-12a-azacyclodecaindene-11,13-dione

Base Information

• Chemical Name: 4b-hydroxy-4b,5,6,7,8,9-hexahydro-10-oxa-12a-azacyclodeca
• Molecular Formula: C₁₅H₁₇NO₄
• Molecular Weight: 275.304

Synonyms:4b-hydroxy-4b,5,6,7,8,9-hexahydro-10-oxa-12a-azacyclodecaindene-11,13-dione

Chemical Property of 4b-hydroxy-4b,5,6,7,8,9-hexahydro-10-oxa-12a-azacyclodeca

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

There total 1 articles about 4b-hydroxy-4b,5,6,7,8,9-hexahydro-10-oxa-12a-azacyclodecaindene-11,13-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phthalic anhydride (85-44-9) → 4b-hydroxy-4b,5,6,7,8,9-hexahydro-10-oxa-12a-azacyclodecaindene-11,13-dione (226992-94-5)

Guidance literature:

Multi-step reaction with 4 steps

1: 2.) KOH / 2.) MeOH

2: 31 percent / K₂CO₃ / dimethylformamide / 16 h / Ambient temperature

3: 73 percent / H₂ / Pd on charcoal / methanol / 16 h / 2250.18 Torr / Ambient temperature

4: 77 percent / K₂CO₃ / H₂O; acetone / 12 h / Irradiation

With potassium hydroxide; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; water; N,N-dimethyl-formamide; acetone;

DOI:10.1021/jo990390b

upstream raw materials:

phthalic anhydride

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