{(N,N-bis(2-(diphenylphosphino)ethyl)-n-propylamine)Ir(η4-cycloocta-1,5-diene)}BPh4

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Chemical Name:{(N,N-bis(2-(diphenylphosphino)ethyl)-n-propylamine)Ir(η4-cycloocta-1,5-diene)}BPh4
CAS No.:130574-11-7
Molecular Formula:C₂₄H₂₀B*C₃₉H₄₇IrNP₂
Molecular Weight:1103.21
Hs Code.:

Synonyms:{(N,N-bis(2-(diphenylphosphino)ethyl)-n-propylamine)Ir(η4-cycloocta-1,5-diene)}BPh4

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Chemical Property of {(N,N-bis(2-(diphenylphosphino)ethyl)-n-propylamine)Ir(η4-cycloocta-1,5-diene)}BPh4

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Technology Process of {(N,N-bis(2-(diphenylphosphino)ethyl)-n-propylamine)Ir(η4-cycloocta-1,5-diene)}BPh4

There total 1 articles about {(N,N-bis(2-(diphenylphosphino)ethyl)-n-propylamine)Ir(η4-cycloocta-1,5-diene)}BPh4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: chloro(1,5-cyclooctadiene)iridium(I) dimer

: 30824-25-0
N,N-bis<2-(diphenylphosphino)ethyl>-n-propylamine

: 143-66-8
sodium tetraphenyl borate

: 130574-11-7
{(N,N-bis(2-(diphenylphosphino)ethyl)-n-propylamine)Ir(η4-cycloocta-1,5-diene)}BPh4

Guidance literature:: In tetrahydrofuran; ethanol; under N2, using Schlenk-tube techniques, addn. of solid PNP to a stirred soln. of Ir-complex in THF at room temp., addn. of NaBPh4 in ethanol; slow evapn., collected on a sintered-glass frit, washed with EtOH and n-pentane, dried in a N2 stream; elem. anal.;

Reference yield: 85.0%

: 130574-11-7
{(N,N-bis(2-(diphenylphosphino)ethyl)-n-propylamine)Ir(η4-cycloocta-1,5-diene)}BPh4

: {(N,N-bis(2-diphenylphosphino)ethyl)-n-propylamineIr(σ,η2-C8H13)}

Guidance literature:: With LiHB(C₂H₅)3; In tetrahydrofuran; under N2, using Schlenk-tube techniques, addn. of LiHBEt3 to a stirred soln. of Ir-complex in THF at room temp., addn. of ethanol; partial evapn., collected on a sintered-glass frit, washed with EtOH and n-pentane, dried in a N2 stream; elem. anal.;

Reference yield: 85.0%

: 130574-11-7
{(N,N-bis(2-(diphenylphosphino)ethyl)-n-propylamine)Ir(η4-cycloocta-1,5-diene)}BPh4

: {(N,,N-bis(2-(diphenylphosphino)ethyl)-N-(2-(diethylamino)ethyl)amine)Ir(σ,η2-C8H13)}

Guidance literature:: With LiHB(C₂H₅)3; In tetrahydrofuran; under N2, using Schlenk-tube techniques, addn. of LiHBEt3 to a stirred soln. of Ir-complex in THF at room temp., addn. of ethanol; partial evapn., collected on a sintered-glass frit, washed with EtOH and n-pentane, dried in a N2 stream; elem. anal.;