Technology Process of C18H26ClN3O4
There total 1 articles about C18H26ClN3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: methanol; sodium tetrahydroborate / tetrahydrofuran / 0 °C
2: triethylamine / dichloromethane / 0.5 h / 0 °C
3: sodium azide / dimethyl sulfoxide / 60 °C
4: palladium on activated charcoal; hydrogen / methanol / 1.5 h / 20 °C / 1520.1 Torr
5: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C
With
methanol; sodium tetrahydroborate; sodium azide; palladium on activated charcoal; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -78 - 20 °C
2: manganese(IV) oxide / dichloromethane / 5 h / 20 °C
3: caesium carbonate / N,N-dimethyl-formamide / 100 °C
4: hydrogenchloride / methanol / 3 h / 20 °C
With
hydrogenchloride; manganese(IV) oxide; lithium aluminium tetrahydride; caesium carbonate;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -78 - 20 °C
2: manganese(IV) oxide / dichloromethane / 5 h / 20 °C
3: caesium carbonate / N,N-dimethyl-formamide / 100 °C
4: hydrogenchloride / methanol / 3 h / 20 °C
5: sodium cyanoborohydride / acetonitrile / 3 h / 0 - 20 °C
With
hydrogenchloride; manganese(IV) oxide; lithium aluminium tetrahydride; sodium cyanoborohydride; caesium carbonate;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
