O-<2-(2,4-Di-tert-pentylphenoxy)hexanoyl>-3-oxo-3-(2,4,6-trichloroanilino)propionamidoxime

Base Information

• Chemical Name: O-<2-(2,4-Di-tert-pentylphenoxy)hexanoyl>-3-oxo-3-(2,4,6-trichloroanilino)propionamidoxime
• CAS No.: 92694-92-3
• Molecular Formula: C₃₁H₄₂Cl₃N₃O₄
• Molecular Weight: 627.051

Synonyms:O-<2-(2,4-Di-tert-pentylphenoxy)hexanoyl>-3-oxo-3-(2,4,6-trichloroanilino)propionamidoxime

Chemical Property of O-<2-(2,4-Di-tert-pentylphenoxy)hexanoyl>-3-oxo-3-(2,4,6-trichloroanilino)propionamidoxime

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Technology Process of O-<2-(2,4-Di-tert-pentylphenoxy)hexanoyl>-3-oxo-3-(2,4,6-trichloroanilino)propionamidoxime

There total 2 articles about O-<2-(2,4-Di-tert-pentylphenoxy)hexanoyl>-3-oxo-3-(2,4,6-trichloroanilino)propionamidoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexanoylchlorid (63059-55-2) + 3-Oxo-3-(2,4,6-trichloroanilino)propionamidoxime (78515-46-5) → O-<2-(2,4-Di-tert-pentylphenoxy)hexanoyl>-3-oxo-3-(2,4,6-trichloroanilino)propionamidoxime (92694-92-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; 1. 5 h/RT 2. 30 min reflux;

DOI:10.1021/jo00200a047

Reference yield:

2-cyano-2',4',6'-trichloroacetanilide (24522-44-9) → O-<2-(2,4-Di-tert-pentylphenoxy)hexanoyl>-3-oxo-3-(2,4,6-trichloroanilino)propionamidoxime (92694-92-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 93 percent / hydroxylamine

2: 84 percent / NEt₃ / tetrahydrofuran / 1. 5 h/RT 2. 30 min reflux

With hydroxylamine; triethylamine; In tetrahydrofuran;

DOI:10.1021/jo00200a047

Reference yield: 82.0%

O-<2-(2,4-Di-tert-pentylphenoxy)hexanoyl>-3-oxo-3-(2,4,6-trichloroanilino)propionamidoxime (92694-92-3) → 5-<-1-(2,4-Di-tert-pentylphenoxy)pentyl>-3-<2-oxo-2-(2,4,6-trichloroanilino)ethyl>-1,2,4,oxadiazole (84104-40-5)

Guidance literature:

In xylene; for 2h; Heating; using Dean-Stark Water separator;

DOI:10.1021/jo00200a047

upstream raw materials:

2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexanoylchlorid

3-Oxo-3-(2,4,6-trichloroanilino)propionamidoxime

2-cyano-2',4',6'-trichloroacetanilide

Downstream raw materials:

5-<-1-(2,4-Di-tert-pentylphenoxy)pentyl>-3-<2-oxo-2-(2,4,6-trichloroanilino)ethyl>-1,2,4,oxadiazole

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