C₂₂H₃₂O₃

Base Information

Chemical Name:C₂₂H₃₂O₃
CAS No.:1577210-18-4
Molecular Formula:C₂₂H₃₂O₃
Molecular Weight:344.494
Hs Code.:

C<sub>22</sub>H<sub>32</sub>O<sub>3</sub>

Synonyms:C₂₂H₃₂O₃

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Chemical Property of C₂₂H₃₂O₃

Chemical Property:

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Technology Process of C₂₂H₃₂O₃

There total 11 articles about C₂₂H₃₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1577209-95-0
C₂₆H₃₈O₄Si

: 1577210-18-4
C₂₂H₃₂O₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: selenium(IV) oxide; tert.-butylhydroperoxide / dichloromethane; water / 16 h / 20 °C / Inert atmosphere

2.1: [Rh(nbd)(diphos-4)]BF₄; hydrogen / tetrahydrofuran / 2 h / 20 °C / 31029.7 Torr

3.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6.33 h / 0 - 20 °C / Inert atmosphere

5.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

6.1: trimethylphosphane; titanium(IV) isopropylate / tetrahydrofuran / 3 h / 70 °C / Inert atmosphere

7.1: cerium(III) chloride heptahydrate / tetrahydrofuran / 0.25 h / 20 °C / Schlenk technique; Inert atmosphere

7.2: 0.25 h / 0 °C / Schlenk technique; Inert atmosphere

8.1: titanium tetrachloride / dichloromethane; toluene / 0.25 h / 0 °C / Inert atmosphere

8.2: 0.5 h / -78 °C / Inert atmosphere

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 36 h / 65 °C / Inert atmosphere

10.1: hydrogen; palladium 10% on activated carbon / methanol / 5 h

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; selenium(IV) oxide; cerium(III) chloride heptahydrate; palladium 10% on activated carbon; [Rh(nbd)(diphos-4)]BF₄; tetrabutyl ammonium fluoride; hydrogen; titanium tetrachloride; sodium hydrogencarbonate; Dess-Martin periodane; trimethylphosphane; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1021/ja413106t

Reference yield:

: 1577209-93-8
C₂₅H₃₆O₅Si

: 1577210-18-4
C₂₂H₃₂O₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 1.5 h / 0 °C / Inert atmosphere

2.1: selenium(IV) oxide; tert.-butylhydroperoxide / dichloromethane; water / 16 h / 20 °C / Inert atmosphere

3.1: [Rh(nbd)(diphos-4)]BF₄; hydrogen / tetrahydrofuran / 2 h / 20 °C / 31029.7 Torr

4.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6.33 h / 0 - 20 °C / Inert atmosphere

6.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

7.1: trimethylphosphane; titanium(IV) isopropylate / tetrahydrofuran / 3 h / 70 °C / Inert atmosphere

8.1: cerium(III) chloride heptahydrate / tetrahydrofuran / 0.25 h / 20 °C / Schlenk technique; Inert atmosphere

8.2: 0.25 h / 0 °C / Schlenk technique; Inert atmosphere

9.1: titanium tetrachloride / dichloromethane; toluene / 0.25 h / 0 °C / Inert atmosphere

9.2: 0.5 h / -78 °C / Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 36 h / 65 °C / Inert atmosphere

11.1: hydrogen; palladium 10% on activated carbon / methanol / 5 h

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; selenium(IV) oxide; n-butyllithium; cerium(III) chloride heptahydrate; palladium 10% on activated carbon; [Rh(nbd)(diphos-4)]BF₄; tetrabutyl ammonium fluoride; hydrogen; titanium tetrachloride; sodium hydrogencarbonate; Dess-Martin periodane; trimethylphosphane; In tetrahydrofuran; methanol; hexane; dichloromethane; water; toluene; 1.1: |Wittig Olefination / 1.2: |Wittig Olefination;
DOI:10.1021/ja413106t

Reference yield:

: 1577210-01-5
C₂₆H₄₀O₅Si

: 1577210-18-4
C₂₂H₃₂O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6.33 h / 0 - 20 °C / Inert atmosphere

3.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

4.1: trimethylphosphane; titanium(IV) isopropylate / tetrahydrofuran / 3 h / 70 °C / Inert atmosphere

5.1: cerium(III) chloride heptahydrate / tetrahydrofuran / 0.25 h / 20 °C / Schlenk technique; Inert atmosphere

5.2: 0.25 h / 0 °C / Schlenk technique; Inert atmosphere

6.1: titanium tetrachloride / dichloromethane; toluene / 0.25 h / 0 °C / Inert atmosphere

6.2: 0.5 h / -78 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 36 h / 65 °C / Inert atmosphere

8.1: hydrogen; palladium 10% on activated carbon / methanol / 5 h

With 2,6-dimethylpyridine; titanium(IV) isopropylate; cerium(III) chloride heptahydrate; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; titanium tetrachloride; sodium hydrogencarbonate; Dess-Martin periodane; trimethylphosphane; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja413106t