N-(2-hydroxyethyl)-C-[3-(2,4,6-trichlorophenylamino)phenyl]methane sulphonamide

Base Information

Chemical Name:N-(2-hydroxyethyl)-C-[3-(2,4,6-trichlorophenylamino)phenyl]methane sulphonamide
CAS No.:1159281-94-3
Molecular Formula:C₁₅H₁₅Cl₃N₂O₃S
Molecular Weight:409.721
Hs Code.:

Synonyms:N-(2-hydroxyethyl)-C-[3-(2,4,6-trichlorophenylamino)phenyl]methane sulphonamide

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Chemical Property of N-(2-hydroxyethyl)-C-[3-(2,4,6-trichlorophenylamino)phenyl]methane sulphonamide

Chemical Property:

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Technology Process of N-(2-hydroxyethyl)-C-[3-(2,4,6-trichlorophenylamino)phenyl]methane sulphonamide

There total 4 articles about N-(2-hydroxyethyl)-C-[3-(2,4,6-trichlorophenylamino)phenyl]methane sulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 1073485-64-9
C-(3-amino-phenyl)-N-(2-hydroxy-ethyl)-methanesulfonamide

: 19393-96-5
2-bromo-1,3,5-trichlorobenzene

: 1159281-94-3
N-(2-hydroxyethyl)-C-[3-(2,4,6-trichlorophenylamino)phenyl]methane sulphonamide

Guidance literature:: With potassium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 150 ℃; for 1h; Microwave irradiation;

Reference yield:

: 58032-84-1
(3-nitrophenyl)methanesulfonyl chloride

: 1159281-94-3
N-(2-hydroxyethyl)-C-[3-(2,4,6-trichlorophenylamino)phenyl]methane sulphonamide

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane / 20 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 750.08 Torr / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

4: potassium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 1 h / 150 °C / Inert atmosphere; microwave irradiation; sealed tube

With pyridine; tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;

Reference yield:

: 1159281-95-4
N-[2-(tert-butyldiphenyl-silanyloxy)ethyl]-C-(3-nitrophenyl)methanesulfonamide

: 1159281-94-3
N-(2-hydroxyethyl)-C-[3-(2,4,6-trichlorophenylamino)phenyl]methane sulphonamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 750.08 Torr / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

3: potassium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 1 h / 150 °C / Inert atmosphere; microwave irradiation; sealed tube

With tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; methanol;