Technology Process of C22H46O3SSi4
There total 8 articles about C22H46O3SSi4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
dichloromethane;
at 20 ℃;
for 6h;
Inert atmosphere;
DOI:10.1002/chem.201102318
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N,N-dimethyl acetamide / dichloromethane / 0 - 45 °C / Inert atmosphere
1.2: 0.25 h / 0 - 20 °C / Inert atmosphere
2.1: di-tert-butoxydiazene / benzene / 3 h / 60 °C / Inert atmosphere
3.1: dmap; triethylamine / dichloromethane / 6 h / 20 °C / Inert atmosphere
With
dmap; N,N-dimethyl acetamide; di-tert-butoxydiazene; triethylamine;
In
dichloromethane; benzene;
DOI:10.1002/chem.201102318
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
2.1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C
3.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
3.2: 4 h / 20 °C
4.1: N,N-dimethyl acetamide / dichloromethane / 0 - 45 °C / Inert atmosphere
4.2: 0.25 h / 0 - 20 °C / Inert atmosphere
5.1: di-tert-butoxydiazene / benzene / 3 h / 60 °C / Inert atmosphere
6.1: dmap; triethylamine / dichloromethane / 6 h / 20 °C / Inert atmosphere
With
dmap; lithium aluminium tetrahydride; N,N-dimethyl acetamide; di-tert-butoxydiazene; potassium tert-butylate; Dess-Martin periodane; triethylamine;
In
tetrahydrofuran; dichloromethane; benzene;
2.1: Dess-Martin oxidation;
DOI:10.1002/chem.201102318
