(4-deutero-2,6-dimethylhept-4-yl) 2,6-dideuterophenyl sulfone

Base Information

Chemical Name:(4-deutero-2,6-dimethylhept-4-yl) 2,6-dideuterophenyl sulfone
CAS No.:1622251-05-1
Molecular Formula:C₁₅H₂₄O₂S
Molecular Weight:271.397
Hs Code.:

Synonyms:(4-deutero-2,6-dimethylhept-4-yl) 2,6-dideuterophenyl sulfone

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Chemical Property of (4-deutero-2,6-dimethylhept-4-yl) 2,6-dideuterophenyl sulfone

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Technology Process of (4-deutero-2,6-dimethylhept-4-yl) 2,6-dideuterophenyl sulfone

There total 5 articles about (4-deutero-2,6-dimethylhept-4-yl) 2,6-dideuterophenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1622251-04-0
2,6-dimethylhept-4-yl 2,6-dideuterophenyl sulfone

: 1622251-05-1
(4-deutero-2,6-dimethylhept-4-yl) 2,6-dideuterophenyl sulfone

Guidance literature:: 2,6-dimethylhept-4-yl 2,6-dideuterophenyl sulfone; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -20 ℃; for 0.166667h; Inert atmosphere;

With water-d2; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.16667h;
DOI:10.1002/ejoc.201402171

Reference yield:

: 3112-85-4
methylphenylsulfonate

: 1622251-05-1
(4-deutero-2,6-dimethylhept-4-yl) 2,6-dideuterophenyl sulfone

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane; tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

1.2: 1.17 h / -78 - 0 °C

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane; tetrahydrofuran / 0.08 h / -30 °C / Inert atmosphere

3.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane; tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

3.2: 1.17 h / -78 - 20 °C

4.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane; tetrahydrofuran / 0.17 h / -20 °C / Inert atmosphere

4.2: 1.17 h / -78 - 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane;
DOI:10.1002/ejoc.201402171

Reference yield:

: 1593772-16-7
3-deuteropent-3-yl phenyl sulfone

: 1622251-05-1
(4-deutero-2,6-dimethylhept-4-yl) 2,6-dideuterophenyl sulfone

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane; tetrahydrofuran / 0.08 h / -78 °C

1.2: 0.42 h / -60 °C

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane; tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

2.2: 1.17 h / -78 - 20 °C

3.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane; tetrahydrofuran / 0.17 h / -20 °C / Inert atmosphere

3.2: 1.17 h / -78 - 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane;
DOI:10.1002/ejoc.201402171