trans-4-propylcyclohexanecarbonyl-tetrakis(N^γ-trichloroethoxycarbonyl)polymyxin B (2-10)

Base Information

• Chemical Name: trans-4-propylcyclohexanecarbonyl-tetrakis(N^γ-trichloroethoxycarbonyl)polymyxin B (2-10)
• CAS No.: 1013029-02-1
• Molecular Formula: C₆₅H₉₄Cl₁₂N₁₄O₂₀
• Molecular Weight: 1816.98

Synonyms:trans-4-propylcyclohexanecarbonyl-tetrakis(N^γ-trichloroethoxycarbonyl)polymyxin B (2-10)

Chemical Property of trans-4-propylcyclohexanecarbonyl-tetrakis(N^γ-trichloroethoxycarbonyl)polymyxin B (2-10)

Chemical Property:

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Technology Process of trans-4-propylcyclohexanecarbonyl-tetrakis(N^γ-trichloroethoxycarbonyl)polymyxin B (2-10)

There total 1 articles about trans-4-propylcyclohexanecarbonyl-tetrakis(N^γ-trichloroethoxycarbonyl)polymyxin B (2-10) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.54%

tetrakis(Nγ-trichloroethoxycarbonyl)polymyxin B (2-10) hydrochloride (1013028-77-7) + trans-4-propyl-cyclohexanecarboxylic acid (38289-27-9) → trans-4-propylcyclohexanecarbonyl-tetrakis(Nγ-trichloroethoxycarbonyl)polymyxin B (2-10) (1013029-02-1)

Guidance literature:

With 4-methyl-morpholine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 1h; pH=7.8;

DOI:10.1248/cpb.55.1724

Reference yield:

trans-4-propylcyclohexanecarbonyl-tetrakis(Nγ-trichloroethoxycarbonyl)polymyxin B (2-10) (1013029-02-1) → trans-4-propylcyclohexanecarbonyl-polymyxin B (2-10) (1013211-28-3)

Guidance literature:

With acetic acid; zinc; at 40 ℃; for 5h;

DOI:10.1248/cpb.55.1724

upstream raw materials:

tetrakis(N^γ-trichloroethoxycarbonyl)polymyxin B (2-10) hydrochloride

trans-4-propyl-cyclohexanecarboxylic acid

Downstream raw materials:

trans-4-propylcyclohexanecarbonyl-polymyxin B (2-10)

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