1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(4-hydroxylphenyl)-3-thienyl]perfluorocyclopentene

Base Information

• Chemical Name: 1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(4-hydroxylphenyl)-3-thienyl]perfluorocyclopentene
• CAS No.: 1360465-90-2
• Molecular Formula: C₂₂H₁₆F₆OS₂
• Molecular Weight: 474.491

Synonyms:1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(4-hydroxylphenyl)-3-thienyl]perfluorocyclopentene

Chemical Property of 1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(4-hydroxylphenyl)-3-thienyl]perfluorocyclopentene

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Technology Process of 1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(4-hydroxylphenyl)-3-thienyl]perfluorocyclopentene

There total 1 articles about 1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(4-hydroxylphenyl)-3-thienyl]perfluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(4-methoxylphenyl)-3-thienyl]perfluorocyclopentene (1021298-64-5) → 1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(4-hydroxylphenyl)-3-thienyl]perfluorocyclopentene (1360465-90-2)

Guidance literature:

With boron tribromide; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1039/c2jm15262b

Reference yield: 88.0%

1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(4-hydroxylphenyl)-3-thienyl]perfluorocyclopentene (1360465-90-2) + C25H22N2O4S → C40H30F6N2O2S2

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 180 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.inorgchem.8b00733

Reference yield: 75.0%

1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(4-hydroxylphenyl)-3-thienyl]perfluorocyclopentene (1360465-90-2) + N-(rhodamine-B)lactamethyl-2-(4-chloromethyl)benzamide (1360465-92-4) → 1-(2,5-dimethyl-3-thienyl)-2-{2-methyl-5-[4-N-(rhodamine-B)lactam-ethyl-2-(4-oxymethyl)benzamyl]phenyl-3-thienyl}perfluorocyclopentene (1360465-89-9)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; for 24h; Reflux;

DOI:10.1039/c2jm15262b

upstream raw materials:

1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(4-methoxylphenyl)-3-thienyl]perfluorocyclopentene

Downstream raw materials:

1-(2,5-dimethyl-3-thienyl)-2-{2-methyl-5-[4-N-(rhodamine-B)lactam-(4-oxymethyl)benzhydrazyl]phenyl-3-thienyl}perfluorocyclopentene

1-(2,5-dimethyl-3-thienyl)-2-{2-methyl-5-[4-N-(rhodamine-B)lactam-ethyl-2-(4-oxymethyl)benzamyl]phenyl-3-thienyl}perfluorocyclopentene

C₂₂H₁₆F₆OS₂

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