ethyl [4-(4-(ethyloxy)-1,3-dioxo-9-{[(trifluoromethyl)sulfonyl]oxy}-1,3-dihydro-2H-benzo[f]isoindol-2-yl)phenyl]acetate

Base Information

• Chemical Name: ethyl [4-(4-(ethyloxy)-1,3-dioxo-9-{[(trifluoromethyl)sulfonyl]oxy}-1,3-dihydro-2H-benzo[f]isoindol-2-yl)phenyl]acetate
• CAS No.: 1114974-28-5
• Molecular Formula: C₂₅H₂₀F₃NO₈S
• Molecular Weight: 551.497

Synonyms:ethyl [4-(4-(ethyloxy)-1,3-dioxo-9-{[(trifluoromethyl)sulfonyl]oxy}-1,3-dihydro-2H-benzo[f]isoindol-2-yl)phenyl]acetate

Chemical Property of ethyl [4-(4-(ethyloxy)-1,3-dioxo-9-{[(trifluoromethyl)sulfonyl]oxy}-1,3-dihydro-2H-benzo[f]isoindol-2-yl)phenyl]acetate

Chemical Property:

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Technology Process of ethyl [4-(4-(ethyloxy)-1,3-dioxo-9-{[(trifluoromethyl)sulfonyl]oxy}-1,3-dihydro-2H-benzo[f]isoindol-2-yl)phenyl]acetate

There total 1 articles about ethyl [4-(4-(ethyloxy)-1,3-dioxo-9-{[(trifluoromethyl)sulfonyl]oxy}-1,3-dihydro-2H-benzo[f]isoindol-2-yl)phenyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl {4-[4-(ethyloxy)-9-hydroxy-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]phenyl}acetate (945562-09-4) + trifluoromethylsulfonic anhydride (358-23-6) → ethyl [4-(4-(ethyloxy)-1,3-dioxo-9-{[(trifluoromethyl)sulfonyl]oxy}-1,3-dihydro-2H-benzo[f]isoindol-2-yl)phenyl]acetate (1114974-28-5)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 1.16h;

Reference yield:

Trimethylboroxine (823-96-1) + ethyl [4-(4-(ethyloxy)-1,3-dioxo-9-{[(trifluoromethyl)sulfonyl]oxy}-1,3-dihydro-2H-benzo[f]isoindol-2-yl)phenyl]acetate (1114974-28-5) → ethyl {4-[4-(ethyloxy)-9-methyl-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]phenyl}acetate (1114974-37-6)

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 20 - 100 ℃;

Reference yield:

pyridine-tri-(1E)-1-propen-1-ylboroxin + ethyl [4-(4-(ethyloxy)-1,3-dioxo-9-{[(trifluoromethyl)sulfonyl]oxy}-1,3-dihydro-2H-benzo[f]isoindol-2-yl)phenyl]acetate (1114974-28-5) → ethyl (4-{4-(ethyloxy)-1,3-dioxo-9-[(1Z)-1-propen-1-yl]-1,3-dihydro-2H-benzo[f]isoindol-2-yl}phenyl)acetate + ethyl (4-{4-(ethyloxy)-1,3-dioxo-9-[(1E)-1-propen-1-yl]-1,3-dihydro-2H-benzo[f]isoindol-2-yl}phenyl)acetate (1114974-31-0)

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 90 ℃; for 1.33h;

upstream raw materials:

ethyl {4-[4-(ethyloxy)-9-hydroxy-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]phenyl}acetate

trifluoromethylsulfonic anhydride

Downstream raw materials:

ethyl {4-[4-(ethyloxy)-9-methyl-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]phenyl}acetate

ethyl (4-{4-(ethyloxy)-1,3-dioxo-9-[(1E)-1-propen-1-yl]-1,3-dihydro-2H-benzo[f]isoindol-2-yl}phenyl)acetate

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