morpholine enamine of 2-(m-methoxyphenyl)cyclohexanone

Base Information

Chemical Name:morpholine enamine of 2-(m-methoxyphenyl)cyclohexanone
CAS No.:75209-39-1
Molecular Formula:C₁₇H₂₃NO₂
Molecular Weight:273.375
Hs Code.:

Synonyms:morpholine enamine of 2-(m-methoxyphenyl)cyclohexanone

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Chemical Property of morpholine enamine of 2-(m-methoxyphenyl)cyclohexanone

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Technology Process of morpholine enamine of 2-(m-methoxyphenyl)cyclohexanone

There total 1 articles about morpholine enamine of 2-(m-methoxyphenyl)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.2%

: 110-91-8,99108-56-2
morpholine

: 15547-89-4
2-(3-methoxyphenyl)cyclohexanone

: 75209-39-1
morpholine enamine of 2-(m-methoxyphenyl)cyclohexanone

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 20h; Heating;
DOI:10.1248/cpb.28.1022

Reference yield:

: 75209-39-1
morpholine enamine of 2-(m-methoxyphenyl)cyclohexanone

: 75209-90-4
N-[1-(3-Methoxy-phenyl)-bicyclo[3.3.1]non-9-yl]-2-phenyl-acetamide

Guidance literature:: Multi-step reaction with 8 steps

1: benzene / 18 h / Heating

2: 2N HCl / benzene / 3 h / Ambient temperature

3: 61.2 percent / TsOH / benzene / 75 h / Heating

4: 1.) hydrazine hydrate, conc. HCl, 2.) KOH / 1.) triethylene glycol, 130 deg C, 7 h, 2.) triethylene glycol, 210 deg C, 4 h

5: 580 mg / conc. HCl / ethanol; diethyl ether / 1.5 h / Ambient temperature

6: 85 percent / NH₂OH*HCl, NaOAc*3H₂O / ethanol / 1 h / Heating

7: 4.6 g / LiAlH₄ / tetrahydrofuran / 3 h / Heating

8: 78.7 percent / K₂CO₃ / tetrahydrofuran; H₂O / 1.5 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; toluene-4-sulfonic acid; hydrazine hydrate; In tetrahydrofuran; diethyl ether; ethanol; water; benzene;
DOI:10.1248/cpb.28.1022

Reference yield:

: 75209-39-1
morpholine enamine of 2-(m-methoxyphenyl)cyclohexanone

: 767580-25-6
1-(m-methoxyphenyl)-9-(methylamino)bicyclo<3.3.1>nonane

Guidance literature:: Multi-step reaction with 9 steps

1: benzene / 18 h / Heating

2: 2N HCl / benzene / 3 h / Ambient temperature

3: 61.2 percent / TsOH / benzene / 75 h / Heating

4: 1.) hydrazine hydrate, conc. HCl, 2.) KOH / 1.) triethylene glycol, 130 deg C, 7 h, 2.) triethylene glycol, 210 deg C, 4 h

5: 580 mg / conc. HCl / ethanol; diethyl ether / 1.5 h / Ambient temperature

6: 85 percent / NH₂OH*HCl, NaOAc*3H₂O / ethanol / 1 h / Heating

7: 4.6 g / LiAlH₄ / tetrahydrofuran / 3 h / Heating

8: 870 mg / sat. aq. NaHCO₃ / CH₂Cl₂ / 4 h / Ambient temperature

9: 1.) LiAlH₄ / tetrahydrofuran; diethyl ether / 15 h / Heating

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium acetate; sodium hydrogencarbonate; toluene-4-sulfonic acid; hydrazine hydrate; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; benzene;
DOI:10.1248/cpb.28.1022