C₂₀H₂₈N₂O

Base Information

Chemical Name:C₂₀H₂₈N₂O
CAS No.:1334476-44-6
Molecular Formula:C₂₀H₂₈N₂O
Molecular Weight:312.455
Hs Code.:

C<sub>20</sub>H<sub>28</sub>N<sub>2</sub>O

Synonyms:C₂₀H₂₈N₂O

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Chemical Property of C₂₀H₂₈N₂O

Chemical Property:

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Technology Process of C₂₀H₂₈N₂O

There total 7 articles about C₂₀H₂₈N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 362603-40-5
1-methyl-2-(3,7,8,9-tetrahydro-pyrano[3,2-e]indol-1-yl)-ethylamine

: 1334476-44-6
C₂₀H₂₈N₂O

: 1334476-55-9
C₂₀H₂₆N₂O

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 18h; under 2280.15 Torr;
DOI:10.1016/j.tetlet.2011.07.058

Reference yield:

: 1269985-67-2
C₁₂H₉NO₂

: 1334476-44-6
C₂₀H₂₈N₂O

: 1334476-55-9
C₂₀H₂₆N₂O

Guidance literature:: Multi-step reaction with 5 steps

1: ammonium acetate; acetic acid / Sonication

2: sodium tetrahydroborate; silica gel / chloroform; isopropyl alcohol

3: bromobenzene / Reflux

4: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C / 2280.15 Torr

5: palladium 10% on activated carbon; hydrogen / ethanol / 18 h / 20 °C / 2280.15 Torr

With sodium tetrahydroborate; palladium 10% on activated carbon; ammonium acetate; hydrogen; silica gel; acetic acid; In bromobenzene; ethanol; chloroform; isopropyl alcohol; 1: Henry reaction / 3: Claisen rearrangement;
DOI:10.1016/j.tetlet.2011.07.058

Reference yield:

: 1334476-33-3
C₁₄H₁₂N₂O₃

: 1334476-44-6
C₂₀H₂₈N₂O

: 1334476-55-9
C₂₀H₂₆N₂O

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate; silica gel / chloroform; isopropyl alcohol

2: bromobenzene / Reflux

3: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C / 2280.15 Torr

4: palladium 10% on activated carbon; hydrogen / ethanol / 18 h / 20 °C / 2280.15 Torr

With sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; silica gel; In bromobenzene; ethanol; chloroform; isopropyl alcohol; 2: Claisen rearrangement;
DOI:10.1016/j.tetlet.2011.07.058