C₅₀H₅₈F₆N₂O₂S₂

Base Information

• Chemical Name: C₅₀H₅₈F₆N₂O₂S₂
• CAS No.: 1232880-74-8
• Molecular Formula: C₅₀H₅₈F₆N₂O₂S₂
• Molecular Weight: 897.145
• Mol file: 1232880-74-8.mol

Synonyms:C₅₀H₅₈F₆N₂O₂S₂

Chemical Property of C₅₀H₅₈F₆N₂O₂S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₀H₅₈F₆N₂O₂S₂

There total 3 articles about C₅₀H₅₈F₆N₂O₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

3,6-bis-(5-bromothiophen-2-yl)-N,N'-bis(dodecyl)-1,4-dioxopyrrolo[3,4-c]pyrrole (1232880-65-7) + 3,4,5-trifluorophenylboronic acid (143418-49-9) → C50H58F6N2O2S2 (1232880-74-8)

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; at 80 ℃; for 24h; Inert atmosphere;

Reference yield:

thiophene-2-carbonitrile (1003-31-2) → C50H58F6N2O2S2 (1232880-74-8)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium tert-butylate / tert-Amyl alcohol

2: potassium carbonate / N,N-dimethyl-formamide

3: N-Bromosuccinimide / chloroform

4: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 24 h / 80 °C / Inert atmosphere

With N-Bromosuccinimide; potassium tert-butylate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tert-Amyl alcohol; ethanol; chloroform; water; N,N-dimethyl-formamide; toluene;

Reference yield:

3,6-dithiophen-2-yl-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione → C50H58F6N2O2S2 (1232880-74-8)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide

2: N-Bromosuccinimide / chloroform

3: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 24 h / 80 °C / Inert atmosphere

With N-Bromosuccinimide; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; chloroform; water; N,N-dimethyl-formamide; toluene;

upstream raw materials:

3,6-bis-(5-bromothiophen-2-yl)-N,N'-bis(dodecyl)-1,4-dioxopyrrolo[3,4-c]pyrrole

3,4,5-trifluorophenylboronic acid

thiophene-2-carbonitrile