methyl 4,6-dideoxy-2,3-di-O-methyl-6-piperidino-4-(N'-phenyl)thioureido-α-D-galactopyranoside

Base Information

Chemical Name:methyl 4,6-dideoxy-2,3-di-O-methyl-6-piperidino-4-(N'-phenyl)thioureido-α-D-galactopyranoside
CAS No.:1607435-17-5
Molecular Formula:C₂₁H₃₃N₃O₄S
Molecular Weight:423.577
Hs Code.:

Synonyms:methyl 4,6-dideoxy-2,3-di-O-methyl-6-piperidino-4-(N'-phenyl)thioureido-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4,6-dideoxy-2,3-di-O-methyl-6-piperidino-4-(N'-phenyl)thioureido-α-D-galactopyranoside

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Technology Process of methyl 4,6-dideoxy-2,3-di-O-methyl-6-piperidino-4-(N'-phenyl)thioureido-α-D-galactopyranoside

There total 7 articles about methyl 4,6-dideoxy-2,3-di-O-methyl-6-piperidino-4-(N'-phenyl)thioureido-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1607435-31-3
C₁₄H₂₈N₂O₄

: 103-72-0
phenyl isothiocyanate

: 1607435-17-5
methyl 4,6-dideoxy-2,3-di-O-methyl-6-piperidino-4-(N'-phenyl)thioureido-α-D-galactopyranoside

Guidance literature:: In methanol; at 20 ℃; for 8h;
DOI:10.1016/j.carres.2013.12.026

Reference yield:

: 1607435-14-2
methyl 4-O-benzoyl-6-deoxy-2,3-di-O-methyl-6-piperidino-α-D-glucopyranoside

: 1607435-17-5
methyl 4,6-dideoxy-2,3-di-O-methyl-6-piperidino-4-(N'-phenyl)thioureido-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: sodium methylate / methanol / 2 h / Reflux

2: dichloromethane; pyridine / 2 h / 0 °C

3: sodium azide / N,N-dimethyl-formamide / 72 h / 45 °C

4: 1.3-propanedithiol / methanol / 72 h / 50 °C

5: methanol / 8 h / 20 °C

With 1.3-propanedithiol; sodium azide; sodium methylate; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2013.12.026

Reference yield:

: C₁₅H₂₆F₃NO₇S

: 1607435-17-5
methyl 4,6-dideoxy-2,3-di-O-methyl-6-piperidino-4-(N'-phenyl)thioureido-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / N,N-dimethyl-formamide / 72 h / 45 °C

2: 1.3-propanedithiol / methanol / 72 h / 50 °C

3: methanol / 8 h / 20 °C

With 1.3-propanedithiol; sodium azide; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2013.12.026