(+/-)-trans-4-(4-fluorophenyl)-1-methyl-2,6-dioxo-piperidine-3-carboxylic acid ethyl ester

Base Information

Chemical Name:(+/-)-trans-4-(4-fluorophenyl)-1-methyl-2,6-dioxo-piperidine-3-carboxylic acid ethyl ester
CAS No.:858938-15-5
Molecular Formula:C₁₅H₂₀FNO₂
Molecular Weight:265.328
Hs Code.:

Synonyms:(+/-)-trans-4-(4-fluorophenyl)-1-methyl-2,6-dioxo-piperidine-3-carboxylic acid ethyl ester

Suppliers and Price of (+/-)-trans-4-(4-fluorophenyl)-1-methyl-2,6-dioxo-piperidine-3-carboxylic acid ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-trans-4-(4-fluorophenyl)-1-methyl-2,6-dioxo-piperidine-3-carboxylic acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (+/-)-trans-4-(4-fluorophenyl)-1-methyl-2,6-dioxo-piperidine-3-carboxylic acid ethyl ester

There total 2 articles about (+/-)-trans-4-(4-fluorophenyl)-1-methyl-2,6-dioxo-piperidine-3-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-{[3-(4-fluorophenyl)-3-methanesulfonyloxy-propyl]-methyl-amino}-propionic acid ethyl ester

: 858938-15-5
(+/-)-trans-4-(4-fluorophenyl)-1-methyl-2,6-dioxo-piperidine-3-carboxylic acid ethyl ester

Guidance literature:: 3-{[3-(4-fluorophenyl)-3-methanesulfonyloxy-propyl]-methyl-amino}-propionic acid ethyl ester; With sodium hydride; In DMF (N,N-dimethyl-formamide); at -15 - 30 ℃; for 20 - 22h;

With ethanol; In DMF (N,N-dimethyl-formamide); for 1h;

Reference yield:

: 858938-17-7
(3S,4R)-trans-3-carboethoxy-4-(4-fluorophenyl)-N-methyl-piperidine(-)-mandelic acid salt

: 858938-15-5
(+/-)-trans-4-(4-fluorophenyl)-1-methyl-2,6-dioxo-piperidine-3-carboxylic acid ethyl ester

Guidance literature:: With sodium carbonate; In water; toluene;

Reference yield:

: 858938-15-5
(+/-)-trans-4-(4-fluorophenyl)-1-methyl-2,6-dioxo-piperidine-3-carboxylic acid ethyl ester

: 105812-81-5
(3S,4R)-trans-4-(4-fluorophenyl)-3-hydroxymethyl-N-methylpiperidine

Guidance literature:: (+/-)-trans-4-(4-fluorophenyl)-1-methyl-2,6-dioxo-piperidine-3-carboxylic acid ethyl ester; With methanol; sodium tetrahydroborate; In tert-butyl alcohol; for 8h; Heating / reflux;

With acetic acid; In methanol; tert-butyl alcohol;

With sodium carbonate; In water;