C₂₀H₁₈FNO₃S

Base Information

Chemical Name:C₂₀H₁₈FNO₃S
CAS No.:1374232-96-8
Molecular Formula:C₂₀H₁₈FNO₃S
Molecular Weight:371.432
Hs Code.:

C<sub>20</sub>H<sub>18</sub>FNO<sub>3</sub>S

Synonyms:C₂₀H₁₈FNO₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₁₈FNO₃S

Chemical Property:

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Technology Process of C₂₀H₁₈FNO₃S

There total 10 articles about C₂₀H₁₈FNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374232-95-7
C₂₆H₃₂FNO₄SSi

: 1374232-96-8
C₂₀H₁₈FNO₃S

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 1374232-96-8
C₂₀H₁₈FNO₃S

Guidance literature:: Multi-step reaction with 10 steps

1.1: copper(l) iodide; copper diacetate / water / 48 h / 100 °C

2.1: polyphosphoric acid / 3 h / 90 °C

3.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C

4.2: 0 - 20 °C

5.1: diethylzinc / hexane; toluene / 0 - 20 °C

6.1: N-Bromosuccinimide / dichloromethane / 1 h / 0 - 20 °C

7.1: boron tribromide / dichloromethane / 1 h / -20 - 0 °C

7.2: Cooling with ice

8.1: triethylamine / dmap / tetrahydrofuran / 10 h / 0 - 20 °C

9.1: piperidine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

10.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

With piperidine; hydrogenchloride; N-Bromosuccinimide; n-butyllithium; diethylzinc; boron tribromide; triethylamine; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine; copper diacetate; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 879-56-1
7-Methoxy-2,3-dihydro-1H-quinolin-4-one

: 1374232-96-8
C₂₀H₁₈FNO₃S

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C

2.2: 0 - 20 °C

3.1: diethylzinc / hexane; toluene / 0 - 20 °C

4.1: N-Bromosuccinimide / dichloromethane / 1 h / 0 - 20 °C

5.1: boron tribromide / dichloromethane / 1 h / -20 - 0 °C

5.2: Cooling with ice

6.1: triethylamine / dmap / tetrahydrofuran / 10 h / 0 - 20 °C

7.1: piperidine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

8.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

With piperidine; hydrogenchloride; N-Bromosuccinimide; n-butyllithium; diethylzinc; boron tribromide; triethylamine; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;