methyl 2-(3-(8-bromooctyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

Base Information

• Chemical Name: methyl 2-(3-(8-bromooctyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate
• CAS No.: 1350707-03-7
• Molecular Formula: C₂₆H₃₁BrN₂O₄
• Molecular Weight: 515.447

Synonyms:methyl 2-(3-(8-bromooctyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

Chemical Property of methyl 2-(3-(8-bromooctyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

Chemical Property:

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Technology Process of methyl 2-(3-(8-bromooctyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

There total 1 articles about methyl 2-(3-(8-bromooctyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

1,8-dibromooctane (4549-32-0) + methyl 2-(2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate (525601-46-1) → methyl 2-(3-(8-bromooctyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate (1350707-03-7)

Guidance literature:

methyl 2-(2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate; With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In acetone; for 1h; Reflux;

1,8-dibromooctane; In acetone; at 20 ℃; for 48h;

DOI:10.1016/j.ejmech.2011.09.032

Reference yield: 67.0%

4-ethoxycarbonylpiperazine (120-43-4) + methyl 2-(3-(8-bromooctyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate (1350707-03-7) → ethyl 4-(8-(3-(2-methoxy-2-oxoethyl)-2,4-dioxo-5,5-diphenylimidazolidin-1-yl)octyl)piperazine-1-carboxylate (1350706-70-5)

Guidance literature:

4-ethoxycarbonylpiperazine; With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In acetone; at 40 - 50 ℃; for 0.5h;

methyl 2-(3-(8-bromooctyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate; In acetone; at 20 - 50 ℃;

DOI:10.1016/j.ejmech.2011.09.032

Reference yield: 5.0%

piperazine (110-85-0) + methyl 2-(3-(8-bromooctyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate (1350707-03-7) → methyl 2-(2,4-dioxo-5,5-diphenyl-1-(8-(piperazin-1-yl)octyl)imidazolidin-3-yl)acetate (1350706-72-7)

Guidance literature:

With potassium carbonate; In acetone; at 40 - 50 ℃; for 5h;

DOI:10.1016/j.ejmech.2011.09.032

upstream raw materials:

1,8-dibromooctane

methyl 2-(2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

Downstream raw materials:

methyl 2-(2,4-dioxo-5,5-diphenyl-1-(8-(piperazin-1-yl)octyl)imidazolidin-3-yl)acetate

ethyl 4-(8-(3-(2-methoxy-2-oxoethyl)-2,4-dioxo-5,5-diphenylimidazolidin-1-yl)octyl)piperazine-1-carboxylate

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