2-methacrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-(2-methacryloyloxy)ethyl)-amino]-ethyl ester

Base Information

Chemical Name:2-methacrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-(2-methacryloyloxy)ethyl)-amino]-ethyl ester
CAS No.:1357264-37-9
Molecular Formula:C₂₇H₃₂N₆O₅S
Molecular Weight:552.654
Hs Code.:

Synonyms:2-methacrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-(2-methacryloyloxy)ethyl)-amino]-ethyl ester

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Chemical Property of 2-methacrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-(2-methacryloyloxy)ethyl)-amino]-ethyl ester

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Technology Process of 2-methacrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-(2-methacryloyloxy)ethyl)-amino]-ethyl ester

There total 4 articles about 2-methacrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-(2-methacryloyloxy)ethyl)-amino]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 760-93-0
methacryloyl anhydride

: 1357264-33-5
N-[5-{bis-(2-hydroxyethyl)-amino}-2-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-butyramide

: 1357264-37-9
2-methacrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-(2-methacryloyloxy)ethyl)-amino]-ethyl ester

Guidance literature:: With pyridine; at 55 ℃;

Reference yield:

: N,N-bis-(2-hydroxyethyl)-m-phenylenediamine hydrochloride

: 1357264-37-9
2-methacrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-(2-methacryloyloxy)ethyl)-amino]-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: calcium carbonate / water / 0.5 h / 20 °C

1.2: 1 h / 20 °C

2.1: acetic acid; propionic acid / 0.25 h / 20 °C

2.2: 0 - 5 °C

2.3: 0 - 20 °C

3.1: pyridine / 55 °C

With pyridine; acetic acid; propionic acid; calcium carbonate; In water;

Reference yield:

: 92-02-4
N,N-bis(2-hydroxyethyl)-3-acetamidoaniline

: 1357264-37-9
2-methacrylic acid 2-[[3-butyrylamino-4-(4-cyano-3-methylisothiazol-5-ylazo)-phenyl]-(2-(2-methacryloyloxy)ethyl)-amino]-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; water / 4 h / Reflux

2.1: calcium carbonate / water / 0.5 h / 20 °C

2.2: 1 h / 20 °C

3.1: acetic acid; propionic acid / 0.25 h / 20 °C

3.2: 0 - 5 °C

3.3: 0 - 20 °C

4.1: pyridine / 55 °C

With pyridine; hydrogenchloride; water; acetic acid; propionic acid; calcium carbonate; In water;