[[5,15-bis(4-allyloxyphenyl)-10-ethynyl-20-(trihexylsilyl)ethynyl]-21H,23H-porphinato]zinc

Base Information

Chemical Name:[[5,15-bis(4-allyloxyphenyl)-10-ethynyl-20-(trihexylsilyl)ethynyl]-21H,23H-porphinato]zinc
CAS No.:1055877-98-9
Molecular Formula:C₆₀H₆₆N₄O₂SiZn
Molecular Weight:968.685
Hs Code.:

Synonyms:[[5,15-bis(4-allyloxyphenyl)-10-ethynyl-20-(trihexylsilyl)ethynyl]-21H,23H-porphinato]zinc

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Chemical Property of [[5,15-bis(4-allyloxyphenyl)-10-ethynyl-20-(trihexylsilyl)ethynyl]-21H,23H-porphinato]zinc

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Technology Process of [[5,15-bis(4-allyloxyphenyl)-10-ethynyl-20-(trihexylsilyl)ethynyl]-21H,23H-porphinato]zinc

There total 1 articles about [[5,15-bis(4-allyloxyphenyl)-10-ethynyl-20-(trihexylsilyl)ethynyl]-21H,23H-porphinato]zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.2%

: 3634-67-1
trihexylsilyl chloride

: 1055877-93-4
[[5,15-bis(4-allyloxyphenyl)-10,20-bis(ethynyl)]-21H,23H-porphinato]zinc

: 1055877-98-9
[[5,15-bis(4-allyloxyphenyl)-10-ethynyl-20-(trihexylsilyl)ethynyl]-21H,23H-porphinato]zinc

Guidance literature:: [[5,15-bis(4-allyloxyphenyl)-10,20-bis(ethynyl)]-21H,23H-porphinato]zinc; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; Inert atmosphere;

trihexylsilyl chloride; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1039/b800063h

Reference yield: 61.0%

: 1055877-98-9
[[5,15-bis(4-allyloxyphenyl)-10-ethynyl-20-(trihexylsilyl)ethynyl]-21H,23H-porphinato]zinc

: 1055877-99-0
[5,5'-(1,3-butyne-1,4-diyl)-bis[10,20-bis[2,6-bis(4-allyoxyphenyl)-15-[(trihexylsilyl)ethynyl]porphinato]]]dizinc

Guidance literature:: [[5,15-bis(4-allyloxyphenyl)-10-ethynyl-20-(trihexylsilyl)ethynyl]-21H,23H-porphinato]zinc; With pyridine; air; N,N,N,N,-tetramethylethylenediamine; In dichloromethane; for 0.25h;

With air; copper(l) chloride; In dichloromethane; for 0.5h;
DOI:10.1039/b800063h