bis((2,6-diisopropylphenyl)imido)bis((2,6-diisopropylphenyl)amido)molybdenum(VI)

Base Information

Chemical Name:bis((2,6-diisopropylphenyl)imido)bis((2,6-diisopropylphenyl)amido)molybdenum(VI)
CAS No.:135707-55-0
Molecular Formula:C₄₈H₇₀MoN₄
Molecular Weight:799.051
Hs Code.:

Synonyms:bis((2,6-diisopropylphenyl)imido)bis((2,6-diisopropylphenyl)amido)molybdenum(VI)

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Chemical Property of bis((2,6-diisopropylphenyl)imido)bis((2,6-diisopropylphenyl)amido)molybdenum(VI)

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Technology Process of bis((2,6-diisopropylphenyl)imido)bis((2,6-diisopropylphenyl)amido)molybdenum(VI)

There total 3 articles about bis((2,6-diisopropylphenyl)imido)bis((2,6-diisopropylphenyl)amido)molybdenum(VI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 161331-85-7
[Li(THF)4][Mo(N-2,6-C₆H₃-i-Pr₂)3Cl]

: 24544-04-5
2,6-diisopropylbenzenamine

: 135707-55-0
bis((2,6-diisopropylphenyl)imido)bis((2,6-diisopropylphenyl)amido)molybdenum(VI)

Guidance literature:: In benzene;
DOI:10.1039/c39950000079

Reference yield: 98.9%

: MoCl2(N(2,6-i-Pr2C6H3))2(1,2-dimethoxyethane)

: lithium (2,6-diisopropylphenyl)amide

: 135707-55-0
bis((2,6-diisopropylphenyl)imido)bis((2,6-diisopropylphenyl)amido)molybdenum(VI)

Guidance literature:: In diethyl ether; Li-compound in ether was added over 30 min to a soln. of complex in ether, the mixt. was stirred at 23°C overnight (N2); volatiles were removed in vac., extd. with n-pentane, crystd. at -30°C;
DOI:10.1016/S0020-1693(02)01271-9

Reference yield: 65.0%

: bis((2,6-diisopropylphenyl)imido)dichloromolybdenum(VI)-tetrahydrofuran

: 135707-55-0
bis((2,6-diisopropylphenyl)imido)bis((2,6-diisopropylphenyl)amido)molybdenum(VI)

Guidance literature:: With lithium (2,6-diisopropylphenyl)amide monoetherate; In pentane; byproducts: LiCl; Ar, stirred for 12 h; filtered; recrystd. (pentane, at -40°C);
DOI:10.1021/om00055a065